025-83701931 设为首页 加入收藏
文章摘要
气相色谱/质谱联用法测定饮用水源水中苯胺类化合物
Method for Aniline and Selected Derivatives Determination in Drink Source Water by GC/MS
  
DOI:
中文关键词: 
英文关键词: 
基金项目:
作者单位
储燕萍 上海市浦东新区环境监测站 
唐莺 上海市浦东新区环境监测站 
韩英 上海市浦东新区环境监测站 
黄敏 上海市浦东新区环境监测站 
摘要点击次数: 1673
全文下载次数: 1888
中文摘要:
      采用液液萃取-气相色谱/质谱联用法测定饮用水源水中19种苯胺类化合物,选择DB-5MS色谱柱,讨论了pH值对回收率的影响。方法在0.500 mg/L~5.00 mg/L范围内线性良好,19种苯胺类化合物的检出限为0.016 μg/L~0.067 μg/L,标准溶液平行测定的RSD为1.2%~13.2%,实际样品加标回收率为59.3%~85.3%。
英文摘要:
      A method for determination of 19 aniline and selected derivatives in drink source water was established by GC/MS using DB-5MS column with liquid liquid extraction. The experimental research found pH influence on the recovery. The results indicated that good linearity was obtained in range from 0.500 mg/L to 5.00 mg/L, detection limits of 19 kinds of aniline and selected derivatives from 0.016 μg/L to 0.067 μg/L, RSD of standard solution from 1.2% to 13.2%, spiked recovery of samples from 59.3% to 85.3%.
查看全文   查看/发表评论  下载PDF阅读器
关闭