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| 微波消解-ICP/MS法同时测定水产品中13种元素 |
| Simultaneous Determination of 13 Elementals in Aquatic Products by Microwave Digestion ICP/MS |
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| DOI： |
| 中文关键词: 微波消解 电感耦合等离子体质谱法 元素分析 水产品 |
| 英文关键词: Microwave digestion Inductively coupled plasma mass spectrometry (ICP/MS) Elemental analysis Aquatic products |
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| 中文摘要: |
| 用硝酸-双氧水体系微波消解，以In、Sc为内标，采用电感耦合等离子体质谱法（ICP/MS）同时测定水产品中V、Cr、Co、Ni、Cu、Zn、As、Se、Cd、Sb、Ba、Tl、Pb等13种元素。各元素的检出限在0.05 ng/g～0.064 μg/g之间，样品平行测定4次的RSD＜5%，鲢鱼样品的加标回收率在81%～117%之间。 |
| 英文摘要: |
| A method was developed to simultaneously determine 13 elementals by microwave digestion-ICP/MS in aquatic products with Cesium and Indium as internal standards. HNO3-H2O2 was used to digest the samples. The method detection limits of the 13 elementals ranged from 0.05 ng/g to 0.064 μg/g and the RSDs of 4 parallel determination were less than 5%. The spiked recoveries of silver carp were between 81% and 117%. |
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