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31.
A simple and robust analytical method was developed to simultaneously detect and quantify 17β-estradiol (E2), estrone (E1), 17β-estradiol-3-sulphate (E2-3S), and estrone-3-sulphate (E1-3S) in aqueous solutions (calcium chloride and artificial urine solutions) and agricultural soils using high performance liquid chromatography and UV detection. The standards for all four compounds were linear in the range of 0.01 to 1.0 μg mL(-1) (n = 6) and 1.0 to 20 μg mL(-1) (n = 6), respectively, with correlation coefficients > 0.999. The on-column limits of detection at an injection volume of 50 μL and S/N (signal: noise) ratio of 3 were: 9.0 ng mL(-1), 10 ng mL(-1), 5.0 ng mL(-1), and 7.0 ng mL(-1) for E2-3S, E1-3S, E2 and E1, respectively. The limit of detection and quantification in artificial urine solution and CaCl(2) solution was 1.0 ng mL(-1) for all four compounds. Method detection limits for the compounds in the 3 soils ranged from 2 to 2.4 ng g(-1) (E2-3S and E1-3S), and 1.0 to 2.9 ng g(-1) (E2 and E1), respectively. 相似文献
32.
Frank F. Scherr Ajit K. Sarmah 《Journal of environmental science and health. Part. B》2013,48(8):763-772
A simple and robust analytical method was developed to simultaneously detect and quantify 17β-estradiol (E2), estrone (E1), 17β-estradiol-3-sulphate (E2-3S), and estrone-3-sulphate (E1-3S) in aqueous solutions (calcium chloride and artificial urine solutions) and agricultural soils using high performance liquid chromatography and UV detection. The standards for all four compounds were linear in the range of 0.01 to 1.0 μg mL?1 (n = 6) and 1.0 to 20 μg mL?1 (n = 6), respectively, with correlation coefficients > 0.999. The on-column limits of detection at an injection volume of 50 μL and S/N (signal: noise) ratio of 3 were: 9.0 ng mL?1, 10 ng mL?1, 5.0 ng mL?1, and 7.0 ng mL?1 for E2-3S, E1-3S, E2 and E1, respectively. The limit of detection and quantification in artificial urine solution and CaCl2 solution was 1.0 ng mL?1 for all four compounds. Method detection limits for the compounds in the 3 soils ranged from 2 to 2.4 ng g?1 (E2-3S and E1-3S), and 1.0 to 2.9 ng g?1 (E2 and E1), respectively. 相似文献
33.
Tyagi Shivani Annachhatre Ajit P. 《Journal of Material Cycles and Waste Management》2023,25(2):733-757
Journal of Material Cycles and Waste Management - For environmental protection, safe disposal of toxic pollutants such as heavy metal is very important since they are regarded as hazardous waste.... 相似文献