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81.
This study was undertaken to ascertain optimal methods of sampling, preserving, separating, and analyzing arsenic species
in potentially contaminated waters. Arsenic species are readily transformed in nature by slight changes in conditions. Each
species has a different toxicity and mobility. The conventional field sampling method using filters of 0.45 μm in size could
overestimate the dissolved arsenic concentrations, as passing suspended particles that can act as a sink or source of arsenic
depending on the site condition. For arsenic species in neutral pH and iron-poor waters, the precipitation can be stable for
up to 3 days without any treatment, but for longer periods, a preservative, such as phosphoric acid, is required. Also, the
analytical procedure must be selected carefully because the levels and hydride generation efficiencies of arsenic in different
species can vary, even for the same amount of arsenic. For arsenic speciation in samples that also include organic species,
a hybrid high-performance liquid chromatography (HPLC) column and inductively coupled plasma mass spectrometry (ICP-MS) gave
the best resolution and lowest detection limits. However, the procedure using a solid phase extraction (SPE) cartridge can
be used economically and conveniently for analyzing samples containing only inorganic arsenic species, such as groundwater,
especially that related to mine activity. 相似文献