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81.
青铜峡铝厂氟污染对广武乡玉米影响的调查分析 总被引:1,自引:0,他引:1
监测了青铜峡铝厂东南方向4.5km的广武乡玉米叶,得知含氟量为43.94-166.1mg/kg,对照样品树新林场玉米叶的含氟均值为13.15mg/kg,广武乡的玉米受到了严重的氟污染,农作物减产严重。 相似文献
82.
高灵敏XRF测定废水中痕量砷 总被引:2,自引:0,他引:2
本文提出了在硫酸介质中,以锌粒还原产生氢化物,溴化铜溶液吸收,微孔滤膜过滤制成薄样,X射线荧光测定水中痕量砷的分析方法。 相似文献
83.
小清河水体和沿岸地下水中有机污染物的监测及其毒性分析 总被引:4,自引:0,他引:4
本文对小清河水体和沿岸地下水中的有机污染物进行了色-质联用分析,共检出有机污染物13类93种。并对其毒性效应进行了分析和评价。 相似文献
84.
85.
A novel analytical method has been established for on-line simultaneous determination of fluorene and acenaphthene,chrysene and benzo[a]anthracene (B[a]A) by polarization synchronous fluoromet.y (PSF) coupled to high performance liquid chromatography (HPLC). The detection limits were: 0.039, 0.046, 0.016 and 0.042 mgL-1 for fluorene, acenaphthene, chrysene and B[a]A, respectively. The proposed method has been successfisily applied to simultaneous determination of these PAHs in environmental air and marine sediment samples. 相似文献
86.
A membrane extraction-gas chromatography method was developed fordetermination of organophosphorus pesticides and related compounds including methamidophos, DDVP, dimethoate, methyl parathion, parathion, thiophosphoric acid trimethyl ester, and thiophosphoramidic acid dimethyl ester in water samples. In thismethod, surface-modified acetic cellulose membranes were used to extract the target analytes in water samples, the extracted analytes were back-extracted into a small amount of methanol, andgas chromatography with pulsed flame photometric detector (GC-PFPD) was used to determine the concentrations of targetanalytes in the extracts. The recoveries obtained for thetarget analytes spiked into the water samples ranged from 66to 94%. The method detection limit for each target analyte was 0.05 g L-1. The method developed in this study had shown the advantages of being cheap, simple, fast, and reliable. It had been used successfully to determine the concentrations of target analytes in river water samples. 相似文献
87.
Determination of Trace Organochlorinated Pesticides and Polychlorinated Biphenyls in Water 总被引:1,自引:0,他引:1
Zou Shichun Zhang Zhanxia Sheng Guoying Min Yushun Fu Jiamo 《Environmental monitoring and assessment》1997,44(1-3):563-568
A modified steam distillation liquid-liquid extraction (SDE) device is developed for the enrichment of trace organochlorinated pesticides (OCPs) and polychlorinated biphenyls (PCBs) in up to one litre of water samples. One ml of n-hexane is sufficient to extract the analytes. The extract can be analysed directly by a capillary gas chromatography-electron capture detector. The recoveries range from 84.6 to 102.3% for OCPs and 80.5 to 106.2% for PCBs, respectively. Matrice materials such as lipids and humic substances were removed by the SDE method from the extract and no further cleanup and concentration steps were needed. 相似文献
88.
Solvent microextraction (SME) was applied to the extraction of polycyclic aromatic hydrocarbons (PAHs) from spiked and real environmental soil samples with different matrices. Soil sample was mixed with 7 mL of acetone and 14 mL of water to allow partitioning of the PAHs from the soil to the liquid phase. A 2 microL octane drop suspended from a microsyringe needle tip was then immersed into the stirred solution-soil mixture for extraction. After an 11 min extraction, the octane drop was withdrawn into the syringe and injected directly into the GC for identification and quantification. The whole analysis procedure took 27 min, with an extraction time of 11 min, and a GC separation time of 16 min. A second extraction could be undertaken whilst the GC is running, hence the GC run time currently limits the sample throughput. In this method, a small amount of organic solvent was used for the extraction process, which produced little waste. The limits of detection for lower molecular weight (< 230) PAHs range from 0.13 to 0.36 mg kg-1, and for higher molecular weight (> 250) PAHs are estimated to be between 0.5 and 1.0 mg kg-1, with RSD values generally under 20%. Due to the small volumes of organic solvent used, the consumable cost per extraction is only US$ 0.12. This is the first report of the application of SME to solid samples, and the first report of the use of SME for the analysis of PAHs. 相似文献
89.
本文对某铀矿职业工人和非职业工人头发中的总β、总α放射性水平和铀、钍含量进行了分析测定.结果表明,该矿工人体内铀和钍的蓄积量均在正常放射性本底水平范围内,从头发中检验未观察到工人体内铀、钍放射性水平有明显的升高. 相似文献
90.
分光光度法测定染色废水的色度 总被引:3,自引:0,他引:3
为消除测定染色废水色度的主观误差,采用分光光度法测定染色废水的色度,与稀释倍数法相比,具有精确,重现性好,适用范围广等特点,PH值对色度的测定有明显影响,控制PH值为7.60,测定色度具有可比性。 相似文献