黄酒中尿素的测定

二乙酰－肟分光光度法是测定黄酒等样品中尿素含量的一种快速、灵敏、简便的方法。样品中的尿素与显色试剂在沸水浴中发色１０￣１５ｍｉｎ后比色测定，显色的线性范围在０￣９μｇ尿素之间。测得的结果中包含了瓜氨酸的含量。样品中酒精和葡萄糖的存在不干扰测定。以标准加入法进行定量，从而使该方法的回收率和重现性大大提高，可满足一般痕量分析的要求。     

Reusability of sewage sludge in clay bricks

Bricks produced from sewage sludge in different compositions were investigated. Results of the tests indicated that the sludge proportion is a key factor in determining the brick quality. Increasing the sludge content results in a decrease in brick shrinkage, bulk density, and compressive strength. Brick weight loss on ignition was mainly due to the contribution of the contained organic matter from the sludge being burnt off during the firing process, as well as inorganic substances found in both clay and sludge. The physical, mechanical, and chemical properties of the bricks that were supplemented with various proportions of dried sludge from 10 to 40wt% and generally complied with the General Specification for Brick as per the Malaysian Standard MS 7.6:1972, which dictates the requirements for clay bricks used in walling in general. A standard leaching test method also showed that the leaching of metals from the bricks is very low.     

标准加入分光光度法测定废水中氨氮

本文将标准加入法运用于分光光度分析中，排除了废水氨氮测定中复杂的基体干扰，操作简便，结果准确，适合于单个或小批量水样的直接测定。     

Modeling of n-butane ignition, combustion, and preflame oxidation in the 20-l vessel

The objective of the study reported herein is to simulate various physical and chemical phenomena accompanying fuel-rich n-butane–oxygen mixture preparation, ignition, preflame oxidation, and combustion in the standard 20-l explosion vessel, by applying mathematical models. Based on the computational fluid dynamics (CFD) simulations of the mixing process and natural convection of the ignition kernel, as well as on the analysis of the detailed reaction mechanism of n-butane oxidation, laminar flame propagation, and self-ignition, possible explanations for the phenomena observed experimentally have been suggested. The results of the study indicate that seemingly inflammable mixtures can become hazardous depending on the mixture preparation procedure and forced ignition timing.     

CALCULATION OF CUMULATIVE PERCENTAGE AT SELECTED PARTICLE SIZES FROM BOTTOM WITHDRAWAL TUBE ANALYSIS

ABSTRACT: A new computation method is developed for the bottom withdrawal tube particle size analysis. A transformation on time scale is introduced so that the cumulative percentage of a selected particle size can be determined from a single continuous Oden cum.     

燃放烟花爆竹对声环境评价的影响

噪声自动监测系统可以对噪声进行长期连续监测。通过对连续两年的北京市自动噪声监测数据进行分析表明,烟花爆竹燃放噪声能够对声功能区环境评价参数昼间等效声级、夜间等效声级及其达标率产生较大影响。尤其是1、2类声功能区影响可使等效声级提高10dB,达标率降低3%。提示有必要把节日的燃放噪声与其他噪声分开,单独分析。     

职业安全卫生标准体系建设初探

职业安全卫生标准体系是企业安全科研生产工作的基础 ,是推广试行职业安全卫生管理体系 (OHSMS)的有效技术支撑条件。笔者通过分析职业安全卫生标准应用的实际 ,探索性地提出建立适应企业职业安全卫生管理、研究以及 OHSMS需要的标准化管理体系 ;论述并研讨该体系建立的思路、原则和查询方法以及应用过程的管理 ;以此为职业安全卫生管理、研究和试行OHSMS奠定基础并提供有益的帮助。     

虹膜识别在肉类食品安全追溯系统中的应用及关键技术研究

为了提高大型动物肉类食品的安全性,在研究肉类食品供应链的安全管理的基础上,将大型动物的虹膜识别技术引入食品供应链管理中,构建基于虹膜识别的大型动物肉类食品安全可追溯系统,达到肉类食品安全信息查询及出现安全问题后的个体溯源的目的。借鉴人眼虹膜识别的相关技术,以牛眼为例对大型动物虹膜识别的相关算法和虹膜定位等关键技术进行研究,运用改进的Sobel算子对图像进行边缘检测;引入二次B样条曲线算法实现了牛眼虹膜的精确定位;分析牛虹膜纹理特征的分布特点,实现了虹膜特征区域的提取及归一化处理。研究成果对大型动物的虹膜识别研究和肉类食品供应链安全管理具有一定的参考意义。     

Transport of simazine in unsaturated sandy soil and predictions of its leaching under hypothetical field conditions

The potential contamination of groundwater by herbicides is often controlled by processes in the vadose zone, through which herbicides travel before entering groundwater. In the vadose zone, both physical and chemical processes affect the fate and transport of herbicides, therefore it is important to represent these processes by mathematical models to predict contaminant movement. To simulate the movement of simazine, a herbicide commonly used in Chilean vineyards, batch and miscible displacement column experiments were performed on a disturbed sandy soil to quantify the primary parameters and processes of simazine transport. Chloride (Cl(-)) was used as a non-reactive tracer, and simazine as the reactive tracer. The Hydrus-1D model was used to estimate the parameters by inversion from the breakthrough curves of the columns and to evaluate the potential groundwater contamination in a sandy soil from the Casablanca Valley, Chile. The two-site, chemical non-equilibrium model was observed to best represent the experimental results of the miscible displacement experiments in laboratory soil columns. Predictions of transport under hypothetical field conditions using the same soil from the column experiments were made for 40 years by applying herbicide during the first 20 years, and then halting the application and considering different rates of groundwater recharge. For recharge rates smaller than 84 mm year(-1), the predicted concentration of simazine at a depth of 1 m is below the U.S. EPA's maximum contaminant levels (4 microg L(-1)). After eight years of application at a groundwater recharge rate of 180 mm year(-1) (approximately 50% of the annual rainfall), simazine was found to reach the groundwater (located at 1 m depth) at a higher concentration (more than 40 microg L(-1)) than the existing guidelines in the USA and Europe.     

Testing the Environmental Kuznets Curve Hypothesis with Bird Populations as Habitat-Specific Environmental Indicators: Evidence from Canada

Abstract:  The traditional environmental Kuznets curve (EKC) hypothesis postulates that environmental degradation follows an inverted U-shaped relationship with gross domestic product (GDP) per capita. We tested the EKC hypothesis with bird populations in 5 different habitats as environmental quality indicators. Because birds are considered environmental goods, for them the EKC hypothesis would instead be associated with a U-shaped relationship between bird populations and GDP per capita. In keeping with the literature, we included other variables in the analysis—namely, human population density and time index variables (the latter variable captured the impact of persistent and exogenous climate and/or policy changes on bird populations over time). Using data from 9 Canadian provinces gathered over 37 years, we used a generalized least-squares regression for each bird habitat type, which accounted for the panel structure of the data, the cross-sectional dependence across provinces in the residuals, heteroskedasticity, and fixed- or random-effect specifications of the models. We found evidence that supports the EKC hypothesis for 3 of the 5 bird population habitat types. In addition, the relationship between human population density and the different bird populations varied, which emphasizes the complex nature of the impact that human populations have on the environment. The relationship between the time-index variable and the different bird populations also varied, which indicates there are other persistent and significant influences on bird populations over time. Overall our EKC results were consistent with those found for threatened bird species, indicating that economic prosperity does indeed act to benefit some bird populations.