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催化极谱法测定降水中微量过氧化氢   总被引:2,自引:0,他引:2  
在0.6mol/L磷酸介质中,钒5-Br-PADAP与H2O2形成三元络合物,于0.05V处产生一极灵敏的极谱波。过氧化氢浓度在0.06-17μg/25mL范围内,峰电流与其含量呈良好线性关系。  相似文献
2.
This paper assessed the composition of waste water effluent generated by a Petrochemical industry and a treatment system developed to improve the quality of the discharge water. Parameters as pH, COD, TSS chloride and lead ions were analysed and treated comparatively using hydrogen peroxide. At pH 8.0 post treatment analysis showed a COD – 96 mg/l TSS – 48 mg/l Cl – 798.75 mg/l and Pb2+ – 2 mg/l for treatment D where 40 g/l of alum was used on 30% solution of H2O2 compared to systems A-C. Process treatment included activated clay with sodium ion resin which at pH 6.8 had COD – 52 mg/l, TSS – 10 mg/l, Cl – 510 mg/l and Pb2+ – 0.070 mg/l. This system has an overall efficiency of 79.0% TSS, 45.83% COD, 97.5% Pb2+ and 36.1% Cl reduction. Characteristics obtained for the study has a higher efficiency compared with FEPA and WHO standard for similar industrial water treatment.  相似文献
3.
Trihalomethanes (THMs) the by-products of chlorination in water treatment are recognised as a threat to public health due to their carcinogenicity. The photodegradation of THMs using hydrogen peroxide has been found to give increased removal efficiency and the outcome of the study may find, its application in designing a unit process for water treatment. Batch experiments were carried out using UV lamp of 83 W and 40% w/w Hydrogen peroxide (H2O2) in test waters between 2.5–10 pH range of chloroform, bromodichloromethane, dibromochloromethane and bromoform at 50–200 μg L−1 initial concentration. 92–100% removal of chloroform, bromodichloromethane, dibromochloromethane and bromoform were found with 0.1% of H2O2 and 90 min of UV exposure.  相似文献
4.
This paper assessed the composition of waste water effluent generated by a Petrochemical industry and a treatment system developed to improve the quality of the discharge water. Parameters as pH, COD, TSS chloride and lead ions were analysed and treated comparatively using hydrogen peroxide. At pH 8.0 post treatment analysis showed a COD – 96 mg/l TSS – 48 mg/l Cl – 798.75 mg/l and Pb2+ – 2 mg/l for treatment D where 40 g/l of alum was used on 30% solution of H2O2 compared to systems A-C. Process treatment included activated clay with sodium ion resin which at pH 6.8 had COD – 52 mg/l, TSS – 10 mg/l, Cl – 510 mg/l and Pb2+ – 0.070 mg/l. This system has an overall efficiency of 79.0% TSS, 45.83% COD, 97.5% Pb2+ and 36.1% Cl reduction. Characteristics obtained for the study has a higher efficiency compared with FEPA and WHO standard for similar industrial water treatment.  相似文献
5.
本文研究了钴(Ⅱ)催化过氧化氢氧化苯基荧光酮的褪色反应,测定了反应级数和表观活化能,建立了测定痕量地的新方法。25℃时本法检出限为29×10-13g/ml,线性范围为0.04~2ng/10ml,催化反应表观活化能为56.15KJ/mol。该方法己用于维生素B12、人发和茶叶中痕量钴的测定.结果满意,相对标准偏差为2.4~3.4%。  相似文献
6.
采用全自动石墨消解仪加热、在碱性条件下用过氧化氢氧化海水中的三价铬,优化了极谱法测定条件,方法检出限为0.20μg/L,加标回收率为82.8%~105%,相对标准偏差<5%,且对有证标准样品测试的结果符合准确度要求。方法具有选择性好、灵敏度高、准确等特点,适用于海水中总铬的测定。  相似文献
7.
为验证大气中SO2的浓度对气态H2O2自动荧光法监测的影响,设置了SO2与H2O2在自动荧光过氧化氢分析仪中的反应实验;同时,利用SO2和H2O2的反应速率公式进行了模拟计算,模拟计算结果与仪器的监测结果基本相符.证明了在大气SO2浓度较高的情况下,气态SO2对H2O2的自动荧光法测定确实会有显著影响,通过模拟计算的方法可对在线监测的H2O2浓度数据进行校正.  相似文献
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