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超临界二氧化碳萃取-GC/MS测定土壤中的多环芳烃 总被引:10,自引:2,他引:10
本文开发了一种采用超临界二氧化碳萃取土壤中多环芳烃、不须经过纯化步骤,直接可用于GC/MS分析的简便、高效的方法。本实验中超临界革取的流体是二氧化碳,改善剂是5%的二氯甲烷/甲醇,萃取温度为120℃、压力为34MPa。GC/MS分析时除了采用外标外,还加入了6种同位素PAHs内标以校正各段PAHs的响应因子。采用本方法成功地测定了我国未开垦森林土壤中的PAHs。 相似文献
3.
用催化吸附 KMnO4溶液吸收化合净化法处理稀土荧光灯生产过程中含汞废气 ,经该工艺处理 ,排放的净化气低于GB162 97 1996《大气污染物综合排放标准》中汞污染物排放标准 相似文献
4.
以水为萃取剂,萃取分离乙醇和环己烷,得到乙醇水溶液和粗环己烷。粗环己煊经精馏提纯,得到纯度为99.91%的纯品;乙醇水溶液经分馏,CaO脱水后得无水乙醇,纯度达99.74%。 相似文献
5.
重金属在牡蛎(Crassostrea virginica)中的生物积累及其影响因素的研究 总被引:11,自引:0,他引:11
牡蛎软体,贝壳和沉积物中Cd、Cr、Cu、Fe、Mn、Pb和Zn等重金属元素被同步分析研究,研究结果表明,重金属在牡蛎中的生物积累是牡自身的新陈代谢、重金属元素的地球化学性质和环境诸因素综合影响的结果,其中牡蛎斩生理作用对重金属在软体中的积累产生的影响尤为重要,而贝壳中重金属的积累对来自环境的影响更为敏感。 相似文献
6.
流行病学调查结果表明,环境的极低频电磁场暴露与人群某些肿瘤,如白血病、乳腺癌、脑肿瘤等,以及生殖、神经、心血管和内分泌等系统疾患的发病相关,这些结果在一定程度上得到实验室人体测试的支持。然而,极低频电磁场对健康影响的确切效应,迄今尚未能作出结论,亟等进一步开展多层次、多水平的研究。 相似文献
7.
支持灾害管理决策的咨询信息系统 总被引:3,自引:0,他引:3
为减少中国大城市灾害造成的损失,运用信息科学、系统科学的方法和计算机技术,建立支持灾害管理决策的咨询信息系统(DMDSCIS)。灾害文献数据库管理系统(DLDBMS)是这一咨询信息系统的知识基础和信息来源。本文论述了“DLDBMS”和三个主要的子系统“灾害文献数据库管理系统”、“灾害事实数据库管理系统”、“中外减灾法规超文本检索系统”的作用、设计思想、构成、功能和实现方法。 相似文献
8.
Janina Seemann Cindy T. González Rodrigo Carballo-Bolaños Kathryn Berry Georg A. Heiss Ulrich Struck Reinhold R. Leinfelder 《Environmental monitoring and assessment》2014,186(3):1747-1763
Environmental and biological reef monitoring was conducted in Almirante Bay (Bahía Almirante) in Bocas del Toro, Panama, to assess impacts from anthropogenic developments. An integrated monitoring investigated how seasonal temperature stress, turbidity, eutrophication and physical impacts threatened reef health and biodiversity throughout the region. Environmental parameters such as total suspended solids [TSS], carbon isotopes (δ13C), C/N ratios, chlorophyll a, irradiance, secchi depth, size fractions of the sediments and isotope composition of dissolved inorganic carbon [DIC] of the water were measured throughout the years 2010 and 2011 and were analysed in order to identify different impact sources. Compared to data from Collin et al. (Smithsonian Contributions to the Marine Sciences 38:324–334, 2009) chlorophyll a has doubled at sites close to the city and the port Almirante (from 0.46–0.49 to 0.78–0.97 μg l?1) and suspension load increased, visible by a decrease in secchi depth values. Visibility decreased from 9-13 m down to 4 m at the bay inlet Boca del Drago, which is strongly exposed to river run off and dredging for the shipping traffic. Eutrophication and turbidity levels seemed to be the determining factor for the loss of hard coral diversity, most significant at chlorophyll a levels higher than 0.5 μg l?1 and TSS levels higher than 4.7 mg l?1. Hard coral cover within the bay has also declined, at some sites down to <10 % with extremely low diversities (7 hard coral species). The hard coral species Porites furcata dominated the reefs in highly impacted areas and showed a strong recovery after bleaching and a higher tolerance to turbidity and eutrophication compared to other hard coral species in the bay. Serious overfishing was detected in the region by a lack of adult and carnivorous fish species, such as grunts, snappers and groupers. Study sites less impacted by anthropogenic activities and/or those with local protection showed a higher hard coral cover and fish abundance; however, an overall loss of hard coral diversity was observed. 相似文献
9.
Temporal variation of Synechococcus, its production (μ) and grazing loss (g) rates were studied for 2 years at nearshore stations, i.e. Port Dickson and Port Klang along the Straits of Malacca. Synechococcus abundance at Port Dickson (0.3–2.3 × 105 cell ml?1) was always higher than at Port Klang (0.3–7.1 × 104 cell ml?1) (p < 0.001). μ ranged up to 0.98 day?1 (0.51 ± 0.29 day?1), while g ranged from 0.02 to 0.31 day?1 (0.15 ± 0.07 day?1) at Port Klang. At Port Dickson, μ and g averaged 0.47 ± 0.13 day?1 (0.29–0.82 day?1) and 0.31 ± 0.14 day?1 (0.13–0.63 day?1), respectively. Synechococcus abundance did not correlate with temperature (p > 0.25), but nutrient and light availability were important factors for their distribution. The relationship was modelled as log Synechococcus = 0.37Secchi ? 0.01DIN + 4.52 where light availability (as Secchi disc depth) was a more important determinant. From a two-factorial experiment, nutrients were not significant for Synechococcus growth as in situ nutrient concentrations exceeded the threshold for saturated growth. However, light availability was important and elevated Synechococcus growth rates especially at Port Dickson (F = 5.94, p < 0.05). As for grazing loss rates, they were independent of either nutrients or light intensity (p > 0.30). In nearshore tropical waters, an estimated 69 % of Synechococcus production could be grazed. 相似文献
10.
Cindy DeForest Hauser Paul Battle Nina Mace 《Atmospheric environment (Oxford, England : 1994)》2009,43(10):1823-1826
Passive sampling devices are popular in applications which do not require the monitoring of hourly concentrations. Nitrogen oxides are often collected using filters coated with 2-phenyl-4,4,5,5-tetramethylimidazoline-1-oxyl-3-oxide (PTIO). The filter extract can then be analyzed using flow injection analysis ion chromatography fitted with a copper/cadmium reduction column or UV–vis spectroscopy. When the latter is used to measure low concentrations of nitrogen oxides, absorbance by PTIO at the analytical wavelength of 545 nm contributes significantly. PTIO concentration on the filter also shows variation with filter storage and exposure time not accounted for in a single point blank subtraction at the analytical wavelength. A method is presented that uses a scaling factor to account for variations in concentration of PTIO on the field blank and provides a more accurate method for determining and correcting for the PTIO contribution to absorption when measuring ambient nitrogen oxide concentrations. 相似文献