Determination of Trace Organochlorinated Pesticides and Polychlorinated Biphenyls in Water |
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| Authors: | Zou Shichun Zhang Zhanxia Sheng Guoying Min Yushun Fu Jiamo |
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| Institution: | (1) Department of Chemistry, Zhongshan University, Guangzhou, 510275, China;(2) State Key Laboratory of Organic Geochemistry, Chinese Academy of Sciences, Guangzhou, 510640, China |
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| Abstract: | A modified steam distillation liquid-liquid extraction (SDE) device is developed for the enrichment of trace organochlorinated pesticides (OCPs) and polychlorinated biphenyls (PCBs) in up to one litre of water samples. One ml of n-hexane is sufficient to extract the analytes. The extract can be analysed directly by a capillary gas chromatography-electron capture detector. The recoveries range from 84.6 to 102.3% for OCPs and 80.5 to 106.2% for PCBs, respectively. Matrice materials such as lipids and humic substances were removed by the SDE method from the extract and no further cleanup and concentration steps were needed. |
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