| 固相萃取-气相色谱法测定地表水和底泥中硝基苯类化合物 |
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| 引用本文： | 王芳,陆梅,梁卫清. 固相萃取-气相色谱法测定地表水和底泥中硝基苯类化合物[J]. 环境监测管理与技术, 2009, 21(6): 50-52 |
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| 作者姓名： | 王芳 陆梅 梁卫清 |
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| 作者单位： | 淮安市环境监测中心站,江苏,淮安,223001;淮安市环境监测中心站,江苏,淮安,223001;淮安市环境监测中心站,江苏,淮安,223001 |
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| 摘 要： | 采用固相萃取-气相色谱法测定地表水和底泥中9种硝基苯类化合物。方法在0mg／L—4.00mg／L范围内线性良好,硝基苯和间-二硝基苯的检出限为0.05mg／L（水样）和0.05mg／kg（底泥）,其余7种硝基苯类化合物的检出限为0.01mg／L（水样）和0.01mg／kg（底泥）,标准溶液平行测定的RSD≤6.5％,地表水和底泥加标回收率分别为85.1％—103％和78.4％—106％。
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| 关 键 词： | 硝基苯类化合物 固相萃取 气相色谱法 地表水 底泥 |
Determ ination ofNitrobenzene Compoundsin Surface W ater and Substrate Sludge by SPE GC |
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| WANG Fang,LU Mei,LIANG Wei-qing. Determ ination ofNitrobenzene Compoundsin Surface W ater and Substrate Sludge by SPE GC[J]. The Administration and Technique of Environmental Monitoring, 2009, 21(6): 50-52 |
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| Authors: | WANG Fang LU Mei LIANG Wei-qing |
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| Affiliation: | ( Huaian Environmental Monitoring Center, Huaian , Jiangsu 223001, China) |
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| Abstract: | The9 kindsofnitrobenzenecompoundswere determinationinsurfacewaterandsubstratesludge bygaschromatography withsolid phase extraction. A good linearity wasin rangefrom 0 mg/L to 4.00 mg/L.The detection limitsofnitrobenzene and mdinitrobenzenewere 0.05 mg/L(watersamples), 0.05 mg/kg(sub stratesludge sample). The detection lim its ofother7 nitrobenzene compounds were 0.01 mg/L(watersamples),0.01 mg/kg(substratesludgesample). Paralleltestresultsofstandard solutions werelessthan 6.5%. Spikerecoveryrangesofwatersamplesandsubstratesludgesamplewerefrom 85.1% to103% and from 78.4% to106% respectively. |
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| Keywords: | Nitrobenzenecompounds SPE GC Surfacewater Substratesludge |
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