| 反相HPLC-电化学检测测定苯酚和苯胺 |
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| 引用本文： | 兰心仁,辛梅华,谢英.反相HPLC-电化学检测测定苯酚和苯胺[J].环境工程,2005,23(6):59-60. |
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| 作者姓名： | 兰心仁 辛梅华 谢英 |
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| 作者单位： | 华侨大学材料学院环科系,福建,泉州,362021;华侨大学材料学院环科系,福建,泉州,362021;华侨大学材料学院环科系,福建,泉州,362021 |
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| 摘 要： | 在此采用反相HPLC安培检测研究了影响苯酚和苯胺分离的各因素,建立了同时分离测定这两种组分的色谱条件。在ShimpackCLCC8柱上,以0.05molLNaH2PO4+0.05mmolLEDTA·2Na(pH5.5)+10%CH3OH作流动相,于E+0.1V处检测,线性范围在0～15μgmL,检测限在ngmL级。
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| 关 键 词： | 反相高效液相色谱法 安培检测 苯酚 苯胺 |
| 收稿时间： | 2005-03-07 |
| 修稿时间： | 2005-03-07 |
DETERMINATION OF PHENOL AND ANILINE BY REVERSE PLC-ELECTROCHEMISTRY |
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| Lan Xinren et al.DETERMINATION OF PHENOL AND ANILINE BY REVERSE PLC-ELECTROCHEMISTRY[J].Environmental Engineering,2005,23(6):59-60. |
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| Authors: | Lan Xinren |
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| Institution: | Lan Xinren et al |
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| Abstract: | The reverse HPLC-Ampere detection was used to study the factors influencing the separation of phenol from aniline; and it was set up that the chromatographic conditions of separating and detecting the two components simultaneously.Taking 0.05 mol/L NaH_2PO_4+ 0.05 mmol/L EDTA·2Na(pH=5.5)+10% CH_3OH as the mobile phase, the detection was done at Shim-pack CLC-C_8 column on the condition of E+0.1 V,whose linear range and detection limit were 0.15 μg/mL and ng/mL respectively. |
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| Keywords: | reverse high-performance liquid chromatography ampere detection phenol and aniline |
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