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水中硝基苯的快速气相色谱测定
引用本文:史平,侯定远.水中硝基苯的快速气相色谱测定[J].环境科学与技术,1999(1):43-45.
作者姓名:史平  侯定远
作者单位:[1]同济大学环境学院 [2]苏州市环境监测中心站
摘    要:直接进水样气相色谱法快速测定水中的硝基苯,分别采用2%QF-1+1.5OV-1ChromosorbWAW-DMCS(80-100目)(Ⅰ)和5%聚乙醇-6000101白色担体(40-60目)(Ⅱ)为固定相的两种不锈钢柱,FID检测器,对硝基苯完成分离,本法进样4μl的检测限为0.25mg/L,能满足应急污染监测的需要。对柱Ⅰ,提出了一种改善分离的方法.

关 键 词:直接进水样气相色谱法  硝基苯  应急监测

Rapid Determination Of Nitrobezene In Water By GC
Shi Ping, Hou Dingyuan.Rapid Determination Of Nitrobezene In Water By GC[J].Environmental Science and Technology,1999(1):43-45.
Authors:Shi Ping  Hou Dingyuan
Institution:Shi Ping; Hou Dingyuan
Abstract:A Rapid GC method for determination of the nitrobezene in water is studied. The water sample is injected directly into the 1102 GC equipped with FID. Two column,packed with 2%QF-1+1. 50V-1 ad-sorbed on chromosorb W AW-DMCS (80~100 mesh) or 5% polyethylene glycol 6000 on 101 white carrier (40~60 mesh) are compared. on the base of exper iments,this method is found to be accurate,rapid and sen-sitive enough for determining nitrobezene in water at ppm levels,and can be applied in emergency monitoring.A modified technique is proposed to improve the seperation of nitrobezene from water.
Keywords:Direct aqueous injection GC Nitrobezene Emergency monitoring
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