便携式气相色谱—质谱联用仪应急现场测定空气中54种VOCs |
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引用本文: | 刘喜,施玉格. 便携式气相色谱—质谱联用仪应急现场测定空气中54种VOCs[J]. 干旱环境监测, 2016, 0(4). DOI: 10.3969/j.issn.1007-1504.2016.04.003 |
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作者姓名: | 刘喜 施玉格 |
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作者单位: | 新疆维吾尔自治区环境监测总站,新疆乌鲁木齐,830011 |
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摘 要: | ![]() 采用Inficon公司的HAPSITE四级杆气质联用仪,建立便携式气相色谱—质谱联用仪应急现场测定空气中54种挥发性有机物。对各种化合物的线性、加标回收率(56.3%~141.1%)、精密度(3.80%~22.69%)、检出限进行了测定,并将该方法运用到实际样品测定中。结果表明,该方法准确可靠、灵敏度好、分析速度快、操作简便,适用于空气中54种挥发性有机物的现场测定。
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关 键 词: | 便携式气相色谱-四级杆质谱联用仪 挥发性有机物 空气 |
On-site Analysis of the 54 Volatile Organic Compounds in the Atmosphere by Portable Gas Chromatography-Mass Spectrometry |
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Abstract: | ![]() A method for on-site analysis the 54 volatile organic compounds ( VOCs) in the atmosphere was established by u-sing portable gas chromatography -mass spectrometry.The linear,recovery (56.3%~141.1%),precision (3.80%~22. 69%) and detection limit of each compound were detected ,and this method was carried out to detect the actual samples .Re-sults shows that the method has good precision and accuracy ,highly sensitivity,digestion thoroughly,simplicity,which is appli-cable to the on-site analysis of the 54VOCs in the atmosphere. |
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Keywords: | portable gas chromatography -mass spectrometry VOCs atmosphere |
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