| PVC包装材料中酞酸酯增塑剂残留的ASE-GC-MS分析 |
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| 引用本文： | 陈军,柳艳,钱玉山.PVC包装材料中酞酸酯增塑剂残留的ASE-GC-MS分析[J].能源环境保护,2006,20(5):14-16. |
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| 作者姓名： | 陈军 柳艳 钱玉山 |
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| 作者单位： | 1. 苏州出入境检验检疫局,江苏,苏州,215004
2. 煤炭科学研究总院杭州环境保护研究所,浙江,杭州,311201 |
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| 摘 要： | 针对PVC包装材料中酞酸酯（PAEs）增塑剂残留，采用加速溶剂萃取（ASE）和GC／MS联用技术分析5种PAEs（DMP，DEP，DBP，BBP，DEHP），结果表明加速溶剂萃取用于PVC包装材料中PAEs的提取，最佳温度条件为120℃，最佳循环次数为3次。方法检出限达到0．1mg／kg，回收率达到95．5％-99．8％；并且具有很好的重现性和精密度。
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| 关 键 词： | 加速溶剂萃取 气-质联用 酞酸酯增塑剂 聚氯乙烯 |
| 文章编号： | 1006-8759(2006)05-0014-03 |
| 修稿时间： | 2006年7月10日 |
GC/MS TESTING METHOD WITH ACCELERATED SOLVENT EXTRACTION FOR PAES IN PVC PACKING MATERIALS |
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| CHEN Jun,LIU Yan,QIAN Yu-shan.GC/MS TESTING METHOD WITH ACCELERATED SOLVENT EXTRACTION FOR PAES IN PVC PACKING MATERIALS[J].Energy Environmental Protection,2006,20(5):14-16. |
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| Authors: | CHEN Jun LIU Yan QIAN Yu-shan |
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| Abstract: | A new instrumental method for the determination of5phthalate esters(DMP,DEP,DBP,BBP,DEHP),using Accelerated Solvent Extraction and Gas Chromgraphy/Mass Spectrastrum is de-scribed.The optimum condition such as extraction temperature,extraction time,and chromatography condition were studied.Limits of dection were0.1mg/kg with recoveries between95.55%and99.8%.Several commercial PVC packing materials were analyzed. |
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| Keywords: | ASE GC/MS PAEs PVC |
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