检测管法与纳氏试剂光度法测定氨氮的比较研究 |
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引用本文: | 王玲玲,王媛媛,王盈,谢志广.检测管法与纳氏试剂光度法测定氨氮的比较研究[J].云南环境科学,2012(1):101-103. |
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作者姓名: | 王玲玲 王媛媛 王盈 谢志广 |
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作者单位: | 河南省环境监测中心,河南郑州450004 |
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基金项目: | 水专项《地表水环境质量特定监测项目分析测试方法优化研究》(2009ZX07527-001). |
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摘 要: | 对氨氮真空玻璃检测管法和纳氏试剂光度法进行检出限、精密度、准确度,以及实际样品测试方面的比较研究。研究表明,氨氮检测管的检出限为0.2mg/L,精密度测定的相对标准偏差为0%~5.75%,准确度测定的加标回收率为93%~124%。检测管法和纳氏剂法同时测定多种实际样品,结果两种方法的相对误差为-37.8%~11.8%,结论:检测管法能够满足半定量测试的需求。
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关 键 词: | 氨氮 真空玻璃检测管法 纳氏试剂光度法 |
A Comparative Study on the Detection Tube Method and the Nessler' s Reagent Spectrophotometry for Determination of Ammonia Nitrogen |
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Institution: | WANG Ling- ling, WANG Yuan -yuan, WANG Ying, XIE Zhi -guang (Henan Provincial Environmental Monitoring Center, Zhengzhou Henan 450004 China) |
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Abstract: | The comparative study was conducted on vacuum glass detection tube methods and the Nessler' s reagent spectrophotometry in respect of detection limit, precision, accuracy and sample testing. It shows that the detection limit of ammonia nitrogen by detection tube is 0. 2mg/L, the relative standard deviation of precision is 0% -5. 75% , and the recovery of standard addition of accuracy is 93% -124%. When testing various actual samples by the two methods, we have found that the relative deviation of both methods is -37. 8% -11. 8%. It is concluded that detection tube method could meet the needs of semi - quantitative test. |
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Keywords: | ammonia nitrogen vacuum glass detection tube method Nessler' s reagent spectrophotometry |
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