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流动注射分光光度法在线分析水中总铁
引用本文:笪海文,洪陵成,刘爱平,孙西艳.流动注射分光光度法在线分析水中总铁[J].环境监测管理与技术,2009,21(4):48-50.
作者姓名:笪海文  洪陵成  刘爱平  孙西艳
作者单位:1. 河海大学环境科学与工程学院,江苏,南京,210098
2. 河海大学环境科学与工程学院,江苏,南京,210098;南京德林环保仪器有限公司,江苏,南京,210001
摘    要:采用流动注射邻菲哕啉分光光度法在线分析水中总铁,考察了显色剂、消解液、酸度、反应盘管长度、载流流量、注样体积、采样时间等因素对试验的影响。方法在0.100mg/L-10.0mg/L范围内线性良好,检出限为0.04mg/L,实际水样平行测定的RSD≤3.7%,加标回收率为95.0%-96.0%。

关 键 词:总铁  流动注射  邻菲啰啉分光光度法  在线分析  水质

The On - line Determ ination ofthe TotalIron in Water by Flow Injection Spectrophotometry
DA Hai-wen,HONG Ling-cheng,LIU Ai-ping,SUN Xi-yan.The On - line Determ ination ofthe TotalIron in Water by Flow Injection Spectrophotometry[J].The Administration and Technique of Environmental Monitoring,2009,21(4):48-50.
Authors:DA Hai-wen  HONG Ling-cheng  LIU Ai-ping  SUN Xi-yan
Institution:1.Environmental Science and Engineering Department;Hohai University;Nanjing;Jiangsu 210098;China;2.Nanjing Delin Environmental Instruments Co.Ltd;Jiangsu 210001;China
Abstract:The method was established for determination of total iron in water by on-line analysis of o- phenanthroline spectrophotometry. The effects to the test were observed in color reveal reagent, digestion solution, acidity, pipeline length, load flow and injective volume of sample. The method achieved following results: good linearity in the range from 0.100 mg/L to 10.0 mg/L, the detection limits 0.04 mg/L, the RSD of the practical samples ≤3.7% , the recoveries from 95.0% to 96.0%.
Keywords:Total iron  Flow injection  O-phenanthroline spectrophotometry  On-line analysis  Water quality  
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