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| 毛细管气相色谱法测定鳌江表层沉积物中五氯酚和六氯苯 | |
| 引用本文： | 陈骥,陈舜湖,张祖麟,李恩临,章岳蓬.毛细管气相色谱法测定鳌江表层沉积物中五氯酚和六氯苯[J].环境监测管理与技术,2008,20(4):40-42. |
| 作者姓名： | 陈骥 陈舜湖 张祖麟 李恩临 章岳蓬 |
| 作者单位： | 1. 苍南县环境监测站,浙江,苍南,325800;清华大学环境科学与工程系,北京,100084 2. 苍南县环境监测站,浙江,苍南,325800 3. 清华大学环境科学与工程系,北京,100084 4. 平阳县环境监测站,浙江,平阳,325400 |
| 摘 要： | 建立了超声波萃取-醋酸酐原位衍生化-毛细管气相色谱同时测定鳌江表层沉积物中五氯酚和六氯苯的方法，优化了试验条件。方法线性范围为5μg／L-200μg／L，五氯酚和六氯苯的检出限均为0．5ng／g，沉积物标准物质的测定值符合质控要求，基质加标的平均回收率分别为77．7％和81．8％。 |
| 关 键 词： | 五氯酚 六氯苯 毛细管 气相色谱法 沉积物 鳌江 |
Determ ination of Trace Pentachlorophenoland Hexachlorobenzenein Surface Sedimentsofthe Aojiang River by Capillary GC |
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| CHEN Ji,CHEN Shun-hu,ZHANG Zhu-lin,LI En-lin,ZHANG Yue-peng.Determ ination of Trace Pentachlorophenoland Hexachlorobenzenein Surface Sedimentsofthe Aojiang River by Capillary GC[J].The Administration and Technique of Environmental Monitoring,2008,20(4):40-42. | |
| Authors: | CHEN Ji CHEN Shun-hu ZHANG Zhu-lin LI En-lin ZHANG Yue-peng |
| Institution: | CHEN Ji , CHEN Shun-hu , ZHANG Zhu-lin , LI En-lin , ZHANG Yue-peng ( 1. CangNan County Environmental Monitoring Station, CangNan, ZheJiang 325800, China ; Department of Environment Science and Engineering, Tsinghua University, BeiJing 100084, China; 3. PingYang County Environmental Monitoring Station, PingYang, ZheJiang 325400, China) |
| Abstract: | A method was established for the ultrasonic extraction-in situ acetic anhydride derivatization and capillary gas chromatography detection of pentachlorophenol （PCP） and hexachlorobenzene （HCB） in surface sediments from the Aojiang river of ZheJiang Province. Experiment conditions were optimized. The results showed the good linearity was achieved in the range from 5 μg/L to 200 μg/L, detection limits of PCP and HCB were 0.5 ng/g. The test results meted the quality control requirement of sediment standard materials. The mean recoveries of matrix were 77.7% and 81.8% separately. |
| Keywords: | Pentachlorophenol Hexachlorobenzene Capillary Gaschromatography Sediments Aojiangriver |
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