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| 土壤中酞酸酯类化合物监测方法的质量控制研究 | |
| 引用本文： | 邓慕,夏新,王伟,马芳,池靖,多克辛.土壤中酞酸酯类化合物监测方法的质量控制研究[J].环境监控与预警,2012,4(1):14-23. |
| 作者姓名： | 邓慕 夏新 王伟 马芳 池靖 多克辛 |
| 作者单位： | 1. 北京科技大学,北京,100083 2. 中国环境监测总站,北京,100012 3. 河南省环境监测中心,河南郑州,450004 |
| 基金项目： | 环保公益性行业科研专项项目（200809140） |
| 摘 要： | 从监测结果控制的角度对近10年的土壤中PAEs监测方法进行了探讨,重点比较了索氏萃取柱净化GC/MS、微波萃取柱净化GC、加速溶剂萃取柱净化GC/MS和加速溶剂萃取GPCGC/MS方法的检出限、精密度和准确度。旨在为中国土壤监测方法的建立提供基础支撑,为开展质量控制工作提供评价依据。 |
| 关 键 词： | 土壤 酞酸酯 监测方法 质量控制 |
| 收稿时间： | 2011/5/19 0:00:00 |
| 修稿时间： | 2011/6/17 0:00:00 |
The Quality Control in the Monitoring Methods for Phthalate esters in Soil |
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| DENG Mu , XIA Xin , WANG Wei , MA Fang , CHI Jing , DUO Ke-xin.The Quality Control in the Monitoring Methods for Phthalate esters in Soil[J].Environmental Monitoring and Forewarning,2012,4(1):14-23. | |
| Authors: | DENG Mu XIA Xin WANG Wei MA Fang CHI Jing DUO Ke-xin |
| Institution: | 1. Beijing Science and Technology University, Beijing 100083, China; 2. China National Environmental Monitoring Center, Beijing 100012, China; 3. Henan Environmental Monitoring Center, Zhengzhou, Henan 450004, China ) |
| Abstract: | The monitoring methods for phthalate esters(PAEs) in soil in recent 10 years was discussed from monitoring results control. The detection limit, precision and accuracy between the four monitoring methods including soxhlet extraction-column purification - GC/MS, microwave extraction-column purification-GC, accelerated solvent extraction-column purification-GC/MS and accelerated solvent extraction - GPC - GC/MS method were compared in this study. This paper aimed to provide basic support for the establishment of soil monitoring method, and offer evaluating basis for the conduct of quality control. |
| Keywords: | Soil Phthalate Esters Monitoring Method Quality Control |
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