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在线蒸馏-无人值守连续流动分析法测定污水中氨氮
引用本文:何青青,窦艳艳,徐荣,唐佳婷.在线蒸馏-无人值守连续流动分析法测定污水中氨氮[J].环境监控与预警,2016,8(3):18-20.
作者姓名:何青青  窦艳艳  徐荣  唐佳婷
作者单位:南京市环境监测中心站,江苏 南京,210013
摘    要:采用在线蒸馏-无人值守连续流动分析法对污水中氨氮进行检测,方法在0.00~10.0 mg/L范围内线性良好,检出限为0.014 mg/L,实际样品测定的相对标准偏差为1.24%~4.15%,加标回收率为93.0%~108%,精密度和准确度均能满足污水中氨氮的测定要求。

关 键 词:氨氮  连续流动分析  在线蒸馏  无人值守
收稿时间:6/7/2015 12:00:00 AM
修稿时间:2016/2/15 0:00:00

Determination of Ammonia Nitrogen in Wastewater by Continuous Flow Analysis with Online Distillation and Unattended System
HE Qing qing,DOU Yan yan,XU Rong,TANG Jia ting.Determination of Ammonia Nitrogen in Wastewater by Continuous Flow Analysis with Online Distillation and Unattended System[J].Environmental Monitoring and Forewarning,2016,8(3):18-20.
Authors:HE Qing qing  DOU Yan yan  XU Rong  TANG Jia ting
Abstract:Ammonia nitrogen in wastewater was determined by continuous flow analysis( CFA) with online distillation and unattended system. This method showed good linearity in the range of 0. 00 to 10. 0 mg/L, and the detection limit was 0. 014 mg/L. The rela-tive standard deviations (RSD) of parallel samples were between 1. 24% and 4. 15%. The recovery rates were between 93. 0% and 108%. The precision and accuracy of this method fulfilled the requirement for the determination of ammonia nitrogen in wastewater.
Keywords:Ammonia nitrogen  Continuous flow analysis  Online distillation  Unattended system
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