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CFCs生产企业废水及产品成分快速检测分析
引用本文:金玲仁,曹方方,颜涛,张存良,李红莉.CFCs生产企业废水及产品成分快速检测分析[J].中国环境监测,2015,31(6):125-128.
作者姓名:金玲仁  曹方方  颜涛  张存良  李红莉
作者单位:山东省环境监测中心站, 山东济南 250101,山东省环境监测中心站, 山东济南 250101,山东省环境监测中心站, 山东济南 250101,山东省环境监测中心站, 山东济南 250101,山东省环境监测中心站, 山东济南 250101
摘    要:采用车载GC-MS技术,建立了顶空-GC-MS方法对CFCs产品组分及排污废水中三氯一氟甲烷、二氯二氟甲烷、四氯化碳等成分进行监测分析,实现了快速鉴定企业是否违规生产CFCs相关产品,对于判定企业是否违规提供技术依据。同时,采用顶空-GC/ECD方法对废水中的四氯化碳进行定量分析,以排查企业是否超标排污。

关 键 词:车载GC-MS  CFCs  四氯化碳  定量分析
收稿时间:2015/3/16 0:00:00
修稿时间:2015/6/23 0:00:00

Rapidly Detection of CFCs in Products and It's Wastewater Produced by Iillegal Companies
JIN Ling-ren,CAO Fang-fang,YAN Tao,ZHANG Cun-liang and LI Hong-li.Rapidly Detection of CFCs in Products and It''s Wastewater Produced by Iillegal Companies[J].Environmental Monitoring in China,2015,31(6):125-128.
Authors:JIN Ling-ren  CAO Fang-fang  YAN Tao  ZHANG Cun-liang and LI Hong-li
Institution:Shandong Environmental Monitoring Centre, Jinan 250101, China,Shandong Environmental Monitoring Centre, Jinan 250101, China,Shandong Environmental Monitoring Centre, Jinan 250101, China,Shandong Environmental Monitoring Centre, Jinan 250101, China and Shandong Environmental Monitoring Centre, Jinan 250101, China
Abstract:To rapidly identify and provide technical assistance for predicating whether the factory is broking laws to produce CFCs, a Headspace-GC-MS method was proposed to rapidly analyze of trichloromonofluoromethane, dichlorodifluoromethane and carbon tetrachloride in the products and effluent discharged by the companies employing the vehicular GC-MSD technology. The headspace-GC-ECD method was used to analyze the concentration of carbon tetrachloride in waste water, to make sure if the monitoring data coincide with the emission standard.
Keywords:vehicular GC-MS  CFCs  carbon tetrachloride  quantitative analysis
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