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超高效液相色谱法测定生活饮用水中的溴氰菊酯
引用本文:王昭申,史礼貌,李刚.超高效液相色谱法测定生活饮用水中的溴氰菊酯[J].干旱环境监测,2014(2):81-83,89.
作者姓名:王昭申  史礼貌  李刚
作者单位:新疆环境监测总站,新疆乌鲁木齐830011
基金项目:新疆维吾尔自治区科技厅高科技项目(201216148)
摘    要:采用反相超高效液相色谱法测定生活饮用水中的溴氰菊酯,并用于实际样品的分析.该方法用二氯甲烷为萃取剂,以甲醇—水(85 /15,V/V)作为流动相,紫外检测器的检测波长为215 nm.该方法在6 min之内可完成生活饮用水中溴氰菊酯的分离及检测,结果表明,该方法线性范围、精密度、加标回收率均符合相关技术要求,适用于水样中溴氰菊酯的测定.

关 键 词:溴氰菊酯  超高效液相  检测  生活饮用水

Determination of Deltamethrin in Domestic Drinking Water by UPLC
WANG Zhao -shen,SHI Li -mao,LI Gang.Determination of Deltamethrin in Domestic Drinking Water by UPLC[J].Arid Environmental Monitoring,2014(2):81-83,89.
Authors:WANG Zhao -shen  SHI Li -mao  LI Gang
Institution:(Xinjiang Environmental Monitoring Centre, Urumqi Xinjiang 830011, China)
Abstract:An analytical method for the analysis of Dehamethrin in domestic drinking water was developed by using methylene chloride for extraction and RP - UPLC for detection. Deltamethrin in domestic drinking water was detected within 6 min. 215 nm were employed as detection wavelength by VWD and CI-13OH-H2O( 85/15, V/V) was used as mobile phase. The results showed that the method had high sensitivity and wide linear range. It was suitable for determination of Deltamethrin in domestic drinking water.
Keywords:Deltamethrin  UPLC  detection  domestic drinking water
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