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气相色谱法测定环境空气中2-甲基吡啶的方法
引用本文:高帅鹏,黄飞,张静,史保贵.气相色谱法测定环境空气中2-甲基吡啶的方法[J].干旱环境监测,2017,31(1).
作者姓名:高帅鹏  黄飞  张静  史保贵
作者单位:河南广电计量检测有限公司,河南 郑州,450001
摘    要:研究建立了活性炭管吸附,甲醇解吸,气相色谱法测定环境空气中2-甲基吡啶的方法。该法的检出限为1.8×10~(-3)mg/m~3,线性相关系数r为0.999 6,精密度RSD为1.3%~2.9%,回收率为82%~84%。该方法简单,干扰较少,结果准确、可靠,重现性好,适用于环境空气中2-甲基吡啶的测定。

关 键 词:气相色谱  2-甲基吡啶  环境空气  活性炭管  解吸

Determination of 2-Picoline in Ambient Air by Gas Chromatography
GAO Shuai-peng,HUANG Fei,ZHANG Jing,SHI Bao-gui.Determination of 2-Picoline in Ambient Air by Gas Chromatography[J].Arid Environmental Monitoring,2017,31(1).
Authors:GAO Shuai-peng  HUANG Fei  ZHANG Jing  SHI Bao-gui
Abstract:A simple and sensitive gas chromatography method for determining 2-Picoline in air ambient was established which activated by carbon tubes and desorpted by methanol.The detect limits of this method is consistently bellowed 1.8×10-3 mg/m3, the linear correlated coefficient(r)is 0.999 6, and with recoveries from are ranged 82% to 84%, and the RSD was between 1.3% and 2.9%.The method is simple,less interference,accurate and highly reproducible, suitable for determining the 2-Picoline in air ambient.
Keywords:gas chromatography  2-Picoline  air  activated carbon tubes  desorb
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