| 快速溶剂萃取—凝胶渗透色谱净化-GC／MS分析土壤中酞酸酯（PAEs） |
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| 引用本文： | 邵昶铭,朱文萍.快速溶剂萃取—凝胶渗透色谱净化-GC／MS分析土壤中酞酸酯（PAEs）[J].干旱环境监测,2009,23(2):73-76. |
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| 作者姓名： | 邵昶铭 朱文萍 |
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| 作者单位： | 甘肃省环境监测中心站,甘肃,兰州,730030 |
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| 摘 要： | 采用毛细管柱气相色谱-质谱选择离子检测技术，结合加速溶剂萃取和凝胶渗透色谱净化方法，分析土壤中的6种酞酸酯类（PAFs）化合物。结果表明，土壤中6种PAEs检出限在14—42μg/kg间，加标平均回收率为65．5％～104．4％，相对标准偏差为5．19％～9．61％。方法具有操作简便、纯化效果好和对环境友好的特点，且具有很强的实用性。
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| 关 键 词： | GC/MS选择离子检测 酞酸酯类化合物 加速溶剂萃取 GPC净化 |
Analysis of Phthalates(PAEs) in Soil Using GC/MS Coupled with Accelerated Solvent Extraction and Gel Permeation Chromatographic Purification |
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| SHAO Chang-ming,ZHU Wen-ping.Analysis of Phthalates(PAEs) in Soil Using GC/MS Coupled with Accelerated Solvent Extraction and Gel Permeation Chromatographic Purification[J].Arid Environmental Monitoring,2009,23(2):73-76. |
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| Authors: | SHAO Chang-ming ZHU Wen-ping |
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| Institution: | SHAO Chang-ming,ZHU Wen-ping(Gansu Environmental Monitoring Center,Lanzhou Gansu 730030,China) |
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| Abstract: | The analytical method of six types of phthalates （PAEs） compounds in soil using capillary column gas chromatographymass spectrometry with selected ion monitor （GC - MS- SIM） coupled with accelerated solvent extraction and gel penniation chromatographic purification has been established. The results indicated that the determination limit of six types of PAEs in soil ranged from 14 μg/kg to 42μg/kg with 65.5% ～ 104.4% average recoveries and 5.19% - 9.61% relative standard deviation. The method with the advantages of simple operation, good purification and more friendly to environment will be of ilranense benefit for practical applications. |
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| Keywords: | GC-MS-SIM phthalates compounds accelerated solvent extraction GPC purification |
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