| 城市生活垃圾中纤维素含量测定方法优化 |
| |
| 引用本文： | 唐建,邱忠平,海维燕,周丽萍,童霏.城市生活垃圾中纤维素含量测定方法优化[J].环境工程学报,2011,5(11):2615-2618. |
| |
| 作者姓名： | 唐建 邱忠平 海维燕 周丽萍 童霏 |
| |
| 作者单位： | 西南交通大学生命科学与工程学院,成都,610031 |
| |
| 基金项目： | 四川省科技厅支撑计划项目(2011SZ0229)；西南交通大学校基金资助项目（2007B10） |
| |
| 摘 要： | 对传统硫酸法进行改进，建立适用于城市生活垃圾纤维素含量的测定方法。以脂肪抽提时间、硫酸浓度、水解反应温度、水解反应时间、稀释硫酸浓度、回流时间为考察因素进行6因素5水平正交实验。结果表明，测定纤维素含量的最佳条件为：脂肪抽提时间4h、硫酸浓度70％、水解反应温度30℃、水解反应时间5h、稀释硫酸浓度5％、回流时间3h。优化后纤维素测定条件RSD均小于1．69％，平均回收率98．76％，表明该方法的精度高，可靠行强。
|
| 关 键 词： | 纤维素 正交实验 优化条件 |
Optimization of determination conditions for cellulose content of municipal solid waste |
| |
| Tang Jian,Qiu Zhongping,Hai Weiyan,Zhou Liping and Tong Fei.Optimization of determination conditions for cellulose content of municipal solid waste[J].Techniques and Equipment for Environmental Pollution Control,2011,5(11):2615-2618. |
| |
| Authors: | Tang Jian Qiu Zhongping Hai Weiyan Zhou Liping and Tong Fei |
| |
| Institution: | Tang Jian Qiu Zhongping Hai Weiyan Zhou Liping Tong Fei (School of Life Science and Engineering,Southwest Jiaotong University,Chengdu 610031,China) |
| |
| Abstract: | On the basis of improving the traditional sulfuric acid method,a measurement was explored to test the content of cellulose in municipal refuse.Orthogonal experiments with six elements plus five levels,including fat extraction time,acid concentration,hydrolysis temperature,hydrolysis reaction time,concentration of dilute sulfuric acid and reflux time,were designed and carried out.The results showed that the optimal conditions for determination of cellulose content were: fat extraction time of 4 h,sulfuric ac... |
| |
| Keywords: | cellulose orthogonal experiments optimum conditions |
| 本文献已被 CNKI 万方数据 等数据库收录！ |
| 点击此处可从《环境工程学报》浏览原始摘要信息 |
| 点击此处可从《环境工程学报》下载免费的PDF全文 |
|
