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超声辐射浸渍法制备Fe-Ni-Mn/Al_2O_3催化剂及性能研究
引用本文:张占梅,何世德,周富春.超声辐射浸渍法制备Fe-Ni-Mn/Al_2O_3催化剂及性能研究[J].环境污染治理技术与设备,2012(1):173-177.
作者姓名:张占梅  何世德  周富春
作者单位:[1]重庆交通大学河海学院,重庆400074 [2]重庆远达水务有限公司,重庆400060
基金项目:科技部科技型中小企业技术创新基金项目(10C26215115002)
摘    要:以Al2O3为载体,分别采用超声辐射浸渍法和普通浸渍方法制备Fe-Ni-Mn/Al2O3催化剂。采用BET、XRD和SEM对催化剂的理化性质和孔结构进行了分析,以模拟酸性绿B废水为研究对象考察催化剂的催化性能。实验结果表明,浸渍溶液pH值和焙烧温度显著影响催化剂的性能。与普通浸渍法相比,超声浸渍法制备的Fe-Ni-Mn/Al2O3催化剂对酸性绿B脱色反应表现出较高的催化活性。

关 键 词:超声辐射  催化剂  Fe-Ni-Mn/Al2O3  催化活性

Preparation of Fe-Ni-Mn/Al_2O_3 catalyst by ultrasonic irradiation impregnation method and its property investigation
Zhang Zhanmei,He Shide Zhou Fuchun.Preparation of Fe-Ni-Mn/Al_2O_3 catalyst by ultrasonic irradiation impregnation method and its property investigation[J].Techniques and Equipment for Environmental Pollution Control,2012(1):173-177.
Authors:Zhang Zhanmei  He Shide Zhou Fuchun
Institution:1.School of River and Ocean Engineering,Chongqing Jiaotong University,Chongqing 400074,China; 2.Chongqing Yuanda Water Service Co.Ltd.,Chongqing 400060,China)
Abstract:In this study,with Al2O3 as the carrier,Fe-Ni-Mn/ Al2O3 catalyst was prepared with ultrasonic irradiation impregnation method and conventional impregnation method separately.The physicochemical properties and microstructure of the catalyst were examined by means of BET,XRD and SEM.With simulated wastewater containing Acid Green B,the catalytic performance of the prepared catalyst was examined.It was found that the pH value of impregnation solution and calcination temperature had significant effect on the properties of this catalyst.Compared with catalyst prepared with conventional impregnation method,Fe-Ni-Mn/Al2O3 catalyst prepared with ultrasonic irradiation impregnation method had higher catalytic activity in the decolorization process of Acid Green B.
Keywords:ultrasonic irradiation  catalyst  Fe-Ni-Mn/Al2O3  catalytic activity
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