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气相色谱法测定废水中6种挥发性脂肪酸含量
引用本文:顾福权,徐红娟,柳展飞,陈罡,滕飞.气相色谱法测定废水中6种挥发性脂肪酸含量[J].能源环境保护,2014(3):62-64.
作者姓名:顾福权  徐红娟  柳展飞  陈罡  滕飞
作者单位:[1]绍兴市水环境科学研究院有限公司,浙江绍兴312000 [2]杭州市萧山区环境保护局,杭州萧山311201
摘    要:挥发性脂肪酸(VFA)是厌氧消化过程的重要中间产物,在反应器运行中,出水VFA用作重要的控制指标。通过色谱条件探索将各种脂肪酸分离,同时研究了水样酸碱度,吸附等对测定的影响,进一步优化了废水中挥发性脂肪酸的测定。方法的检出限在0.99~1.77 mg/L,回收率在90.9%~102.7%之间,相对标准差(n=5)在1.3%~3.8%之间。

关 键 词:气相色谱  废水  挥发性脂肪酸

CONTENT OF 6 VOLATILE FATTY ALIDI OF WASTEWATEI BY GAS CHROMATO GRAPHY C GC
GU Fu-quan,XU Hong-juan,LIU Zhan-fei,CHEN Gang,TENG Fei.CONTENT OF 6 VOLATILE FATTY ALIDI OF WASTEWATEI BY GAS CHROMATO GRAPHY C GC[J].Energy Environmental Protection,2014(3):62-64.
Authors:GU Fu-quan  XU Hong-juan  LIU Zhan-fei  CHEN Gang  TENG Fei
Institution:1.Shaoxing Water Environmental Science Reserld lnstinte, Ltd, Shaoxing 312000, China; 2.Environmental Protection Bureau Of Xiaoshan District, Hangzhou 311201, China)
Abstract:VFA is an important intermediate material in anaerobic digestion. VFA is a major index during the process. Separating the fatty acid by chromatographic conditions, and studying how the water's PH, andadsorption influnce the tests, it optimizes the test. Detection limits found were in the range of 0.99-1.77 mg·L-1. Values of recovery found were ranged form 90.9%-102.7%,RSD's(n=5) range form 1.3% -3.8%.
Keywords:gas chromatography  waste water  VFA
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