| 稻、土及田水中锐劲特残留量分析方法 |
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| 引用本文： | 陆贻勇,周培,等.稻、土及田水中锐劲特残留量分析方法[J].上海环境科学,2001,20(10):499-501. |
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| 作者姓名： | 陆贻勇 周培 |
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| 作者单位： | 陆贻通（上海交通大学农业环境生态研究所，上海 201101）;周培（上海交通大学农业环境生态研究所，上海 201101）;吴银良（上海交通大学农业环境生态研究所，上海 201101） |
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| 摘 要： | 建立了新型杀虫剂锐劲特及其代谢物在水稻、土壤、田水中的气相色谱毛细管柱残留分析方法。该方法对锐劲特及其代谢物MB46513、MB45950、MB46136、RPA200766等，在水稻中的最低检出浓度依次为：0.002,0.001,0.001,0.004,0.01mg/kg；在土壤中这几种组分最低检出浓度为水稻中的1／3；在田水中最低检出浓度为水稻中的1／25。加标回收率83.4%-97.7%。变异系数1.86%-7.07%。
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| 关 键 词： | 农药残留量 锐劲特 水稻 土壤 田水 残留分析 杀虫剂 水质 农药污染监测 |
| 修稿时间： | 2001年3月27日 |
Analytical Method of Fipronil Residue in Rice, Soil and Water |
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| Lu Yitong Zhou Pei Wu Yingliang.Analytical Method of Fipronil Residue in Rice, Soil and Water[J].Shanghai Environmental Science,2001,20(10):499-501. |
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| Authors: | Lu Yitong Zhou Pei Wu Yingliang |
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| Abstract: | Analytical method of fipronil residue and its metabolites in rice, soil and water by capillary column gas chroma-tography has been established. The detection limits of fipionil and its metabolites MB46513, MB45950, MB46136 and RPA 20076etc. were 0.002, 0.001, 0.001, 0.004 and 0.01mg/kg respectively, and in.soil, its detection limit were 1/3 of rice, and 1/25 of water, recovery rates were 83.4%-97.7%, with average coefficiency of variation 1.86%-7.07%. |
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| Keywords: | Pesticide residue Fipronil Rice Soil Water Residue analysis |
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