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热脱附/毛细管气相色谱/质谱法测定车内空气中挥发性有机物
引用本文:穆肃,周春宏.热脱附/毛细管气相色谱/质谱法测定车内空气中挥发性有机物[J].环境科学与管理,2009,34(3):148-150.
作者姓名:穆肃  周春宏
作者单位:江苏省环境监测中心,江苏,南京,210036
摘    要:建立了热脱附/毛细管气相色谱/质谱联用测定车内空气中苯、甲苯、乙酸丁酯、乙苯、对/间二甲苯、苯乙烯、邻二甲苯、十一烷和对二氯苯等挥发性有机物采样、分析方法。十种挥发性有机物在一定浓度范围内工作曲线线性良好,相关系数均在0.9970~0.9998之间。检出限在0.2~1.2μg/m^3。用该法检测了某汽车企业生产的轿车内的空气,取得满意结果,表明本方法具有一定的实用性、推广性。

关 键 词:车内空气  热脱附  挥发性有机物  气相色谱/质谱

Determination of Volatile Organic Compounds(VOCs) in Car Air Using Thermal Desorption by Gas Chromatography/Mass Spectrometry(GC/MS)
Mu Su,Zhou Chunhong.Determination of Volatile Organic Compounds(VOCs) in Car Air Using Thermal Desorption by Gas Chromatography/Mass Spectrometry(GC/MS)[J].Environmental Science and Management,2009,34(3):148-150.
Authors:Mu Su  Zhou Chunhong
Institution:Environmental Monitoring Center of Jiangsu Province;Nanjing 210036;China
Abstract:A method has been developed for the confirmation and quantitation of ten VOCs including benzene, toluene, butyl acetate, ethylbenzene, m/p - xylene, styrene, o - xylene1,4 - dichlorobenzene, undecane. This method extract VOCs from in - car air using Tenax - TA Adsorbent Cartridge. The concentration of VOCs is determined using thermal Jesorption by gas chromatography/mass spectrometry (GC/MS). The limit of detection (LOD) was 0. 2 - 1.2μg/m^3. The optimized method has been -sncessfully applied to the analysis of field samples from in -car air.
Keywords:in-car air  thermal desorption  VOCs  GC/MS[1]  
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