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吹扫捕集-气相色谱法测定水中丙烯腈、丙烯醛
引用本文:张建萍,王臻,谢争.吹扫捕集-气相色谱法测定水中丙烯腈、丙烯醛[J].环境科学与管理,2011,36(3):100-101,153.
作者姓名:张建萍  王臻  谢争
作者单位:上海市环境监测中心,上海,200030
摘    要:采用吹扫捕集-气相色谱测定水中丙烯腈、丙烯醛,优化试验条件。该方法具有较高的灵敏度、良好的线性、方法简便。丙烯腈检出限为0.002 mg/L;丙烯醛检出限为0.003 mg/L,标准样品测定的相对标准偏差为3.2%,实际样品的加标回收率为80.0%~110%。

关 键 词:丙烯腈  丙烯醛  气相色谱法  吹扫捕集

Determination of Acrylonitrile,Acrolein in Water by GC with Purge and Trap
Zhang Jianping,Wang Zhen,Xie Zheng.Determination of Acrylonitrile,Acrolein in Water by GC with Purge and Trap[J].Environmental Science and Management,2011,36(3):100-101,153.
Authors:Zhang Jianping  Wang Zhen  Xie Zheng
Institution:(Shanghai Environment Monitoring Center, Shanghai 200030, China)
Abstract:The method is established to determine acrylonitrile and acrolein in Water by purge and trap - Gas Chromatography. It is a method with high sensitivity, good linearity, lower detect limit and can be easily operated as well. The detect limit of Aerylonitrile is 0. 002 mg/L while the hmit of Acrolein is 0. 003 mg/L. The relative standard deviation when analyzing a standard sample runs at 3.2% and it has a 80% - 110% rate of recovery.
Keywords:aerylonitrile  aerolein  gas chromatography  purge and trap
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