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恒能量同步荧光光谱法测定水体中多环芳烃
引用本文:何立芳,章汝平,陈杰斌,林水东.恒能量同步荧光光谱法测定水体中多环芳烃[J].环境科学与技术,2011,34(1):96-99.
作者姓名:何立芳  章汝平  陈杰斌  林水东
作者单位:龙岩学院化学与材料工程系,福建龙岩,364000
基金项目:福建省科技厅科技计划重点项目,福建省自然科学基金,福建省科技厅省属高校基金,福建省教育厅科学研究项目
摘    要:建立了胶束溶液中多环芳烃混合物同时测定的恒能量同步荧光分析法,方法简便快速,无需对混合物进行分离,就可实现11种组分的同时鉴别和定量测定,方法的检出限在1.3×10-11~4×10-9g/mL,标准偏差为1.03~1.73,方法应用于分析河水样、污水样中的多环芳烃的效果良好,回收率分别为77.88%~120.13%、6...

关 键 词:多环芳烃  恒能量同步荧光光谱法  胶束溶液

Determination of Polycyclic Aromatic Hydrocarbon in Water By Constant-Energy Synchronous Fluorescence Spectrometry
HE Li-fang,ZHANG Ru-ping,CHEN Jie-bin,LIN Shui-dong.Determination of Polycyclic Aromatic Hydrocarbon in Water By Constant-Energy Synchronous Fluorescence Spectrometry[J].Environmental Science and Technology,2011,34(1):96-99.
Authors:HE Li-fang  ZHANG Ru-ping  CHEN Jie-bin  LIN Shui-dong
Institution:HE Li-fang,ZHANG Ru-ping,CHEN Jie-bin,LIN Shui-dong(Department of Chemistry and Materials Engineering,Longyan Institute,Longyan 364000,China)
Abstract:This paper refers to a new simple constant-energy synchronous fluorimetric method used to determine multi-component polycyclic aromatic hydrocarbons in the mixture of micellar solution(SDS),which can realize the identification and measurement of as many as 11 components in the solution simultaneously without any pretreatment viz.separation of the mixture.It is reported that the range of detection limits was 1.3×1011~4.4×10-9 g/mL;range of standard deviations was 1.03~1.73,the recovery 77.88%~120.13% when analyzing river water and 62.36%~123.56% when analyzing wastewater.
Keywords:polycyclic aromatic hydrocarbons(PAHs)  constant-energy synchronous fluorescence spectroscopy  micelle  
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