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异丙醇助水热法制备钛酸铋粉体的光催化性能
引用本文:刘潘,刘红,徐文婷,滕洪辉.异丙醇助水热法制备钛酸铋粉体的光催化性能[J].环境科学与技术,2009,32(12).
作者姓名:刘潘  刘红  徐文婷  滕洪辉
作者单位:1. 吉林师范大学环境工程学院,吉林,四平,136000
2. 武汉科技大学资源与环境工程学院,湖北,武汉,430081
基金项目:湖北省耐火材料与高温陶瓷重点实验室一省部共建国家重点实验室培育基地开放基金项目资助 
摘    要:以B(iNO)3·35H2O和T(iSO)42为反应物,用异丙醇助水热法制备了钛酸铋光催化剂,并研究不同水热温度和水热时间对样品光催化活性的影响。用XRD表征了样品的结构,UV-vis漫反射测试显示含有Bi12TiO20的样品的吸收带发生了红移,BET测试表明样品的比表面积远远高于化学溶剂分解法制备的钛酸铋的比表面积。以甲基橙为模拟污染物,评价了样品的光催化性能,发现当水热反应温度为140℃,水热反应时间为2.5h时,样品的光催化活性最高,且超过P25。

关 键 词:光催化剂  钛酸铋  水热法  异丙醇  低温

Photocatalytic Activity of Isopropanol-assisted Hydrothermal Synthesizing Bismuth Titanate Powders
LIU Pan,LIU Hong,XU Wen-ting,TENG Hong-hui.Photocatalytic Activity of Isopropanol-assisted Hydrothermal Synthesizing Bismuth Titanate Powders[J].Environmental Science and Technology,2009,32(12).
Authors:LIU Pan  LIU Hong  XU Wen-ting  TENG Hong-hui
Institution:LIU Pan1,LIU Hong2,XU Wen-ting2,TENG Hong-hui1 (1.School of Environmental Engineering,Jilin Normal University,Siping 136000,China,2.School of Resource and Environment,Wuhan University of Science and Technology,Wuhan 430081,China)
Abstract:Photocatalyst of bismuth titanate was synthesized by using B(iNO)33.5H2O and T(iSO)42 as reactants via an isopropanolassisted hydrothermal method,the influence of different hydrothermal temperatures and different hydrothermal times were studied. The structures of samples were characterized by XRD,and UV -vis absorption spectra results revealed that the samples containing Bi12TiO20 red-shifted,BET testing result showed that surface area of as-prepared sample was higher than that prepared by chemical solution...
Keywords:photocatalyst  bismuth titanate  hydrothermal method  isopropanol  low temperature
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