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| 水热法制备N掺杂纳米TiO2及其光催化活性研究 | |
| 引用本文： | 黄雪锋,唐玉朝,黄显怀,桂和荣.水热法制备N掺杂纳米TiO2及其光催化活性研究[J].环境化学,2006,25(1):16-19. |
| 作者姓名： | 黄雪锋 唐玉朝 黄显怀 桂和荣 |
| 作者单位： | 1. 安徽理工大学资源与环境工程系,淮南,232001;安徽建筑工业学院环境工程系,合肥,230022 2. 安徽建筑工业学院环境工程系,合肥,230022 3. 安徽理工大学资源与环境工程系,淮南,232001 |
| 基金项目： | 中国科学院资助项目 , 安徽省高校青年教师科研项目 |
| 摘 要： | 以钛酸四丁酯和氨水为前驱物,采用水热法制备N掺杂TiO2纳米微粒,利用X射线衍射(XRD)、X射线光电子能谱(XPS)、紫外可见漫反射光谱(UV-Vis DRS)等技术对不同条件下制备的产物进行了表征.探讨了不同体积比的前驱物、水热温度、水热时间及煅烧温度对水热产物的影响;考察了N掺杂催化剂在紫外线和可见光下光催化降解甲基橙和苯酚的催化性能. |
| 关 键 词： | 水热法 N掺杂 光催化 |
| 收稿时间： | 2005-03-10 |
| 修稿时间： | 2005-03-10 |
PREPARATION OF NITROGEN DOPED TiO2 NANOSIZE PARTICLES BY HYDROTHERMAL METHOD AND ITS PHOTOCATALYTIC PROPERTIES |
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| HUANG Xue-feng,TANG Yu-chao,HUANG Xian-huai,GUI He-rong.PREPARATION OF NITROGEN DOPED TiO2 NANOSIZE PARTICLES BY HYDROTHERMAL METHOD AND ITS PHOTOCATALYTIC PROPERTIES[J].Environmental Chemistry,2006,25(1):16-19. | |
| Authors: | HUANG Xue-feng TANG Yu-chao HUANG Xian-huai GUI He-rong |
| Abstract: | Nitrogen doped TiO_ 2 nanosize particles were prepared under hydrothermal condition with tetra-n-butyl titanate and ammonia as the precursors.The products obtained under different conditions were characterized by means of X-ray diffraction(XRD),X-ray photoelectron spectroscopy(XPS) and ultraviolet-visible diffuse reflection spectrum(UV-Vis DRS). The influences of various proportion by volume, hydrothermal temperature, hydrothermal time and calcination temperature to the structure and activities of catalysts were investigated. Photocatalytic activities of the nitrogen doped catalysts were evaluated under ultraviolet and visible light irradiation by photodegradation of methylic-orange and phenol respectively. |
| Keywords: | hydrothermal nitrogen doped photocatalysis |
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