共查询到11条相似文献,搜索用时 62 毫秒
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洞庭湖流域土壤中有机氯杀虫剂的残留规律研究 总被引:2,自引:1,他引:2
2004年5月采集了洞庭湖流域45个土壤样品,用AES萃取技术,使用GC/MS方法测定了样品中的六氯笨、滴滴涕(DDTs)、氯丹、艾氏剂、狄氏剂、异狄氏剂、七氟和灭蚁灵.结果表明,六氯苯、滴滴涕的检出率为100%,氯丹和灭蚁灵的检出率很低,艾氏剂、狄氏剂、异狄氏剂和七氯未检出.总有机氯杀虫剂残留量平均值216.24μg/k,其中滴滴涕214.7μg/kg,占总OCPs的99.3%,且有些土壤样品中w(DDT)/w(DDE DDD)值较大,说明DDTs曾作为湘江流域的主要杀虫剂在洞庭湖流域土壤中广泛施用过,并且近期内仍然有输入.六氯苯的残留量虽然较低,但其施用范围广泛.总OCPs在棉田中的残留量很高,在茶场土壤中最低,表明棉田土壤曾因为各种原因施用过大量的有机氯杀虫剂,茶场土壤中有机氯农药的残存量处于安全范围. 相似文献
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气相色谱法同时分析测定土壤中15种有机氯农药残留 总被引:3,自引:1,他引:3
采用石油醚+丙酮(3+1,V/V)作为提取溶剂、硫酸钠溶液与弗罗里藻土净化,气相色谱法同时测定贵州150个土壤背景点15种有机氯农药残留.峰面积与保留时间的精密度分别为1.14~5.15,0.01~0.09;线性关系均在0.99以上;加标回收率为84.3%~127.8%;方法检出限为0.003~0.025ng/g.该方法适用于土壤背景点有机氯农药残留量的分析. 相似文献
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通过对加速溶剂萃取、平行蒸发及净化方法等环节的优化实验,建立了加速溶剂萃取-凝胶净化色谱-气相色谱质谱法测定农用地土壤中23种有机氯农药的检测方法。结果表明,方法检出限为0.0034~0.0052 mg/kg;对化合物质量分数为0.25 mg/kg的土壤加标样品进行平行实验,回收率为82.0%~93.7%;测定结果的相对标准偏差(RSD)≤8.7%。对土壤有证标准质控样品进行分析,测定结果均在验收范围之内。该方法准确可靠,灵敏度较高,样品净化效果较好,能够满足农用地土壤中有机氯农药残留痕量分析的要求。 相似文献
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Persistent Organochlorine Pesticide Residues in Soil and Surface Water of Northern Indo-Gangetic Alluvial Plains 总被引:1,自引:0,他引:1
This study reports the concentration levels and distribution pattern of the organochlorine pesticide (OCPs) residues in the
soil and surface water samples collected from the northern Indo-Gangetic alluvial plains. A total of 31 soil and 23 surface
water samples were collected from the study region in Unnao district covering an area of 2150 km2 and analyzed for aldrin, dieldrin, endrin, HCB, HCH isomers, DDT isomers/metabolites, endosulfan isomers (α and β), endosulfan
sulfate, heptachlor and its metabolites, α-chlordane, γ-chlordane and methoxychlor. In both the soil and surface water samples
β- and δ-isomers of HCH were detected most frequently, whereas, methoxychlor was the least detected pesticide. The results
showed contamination of soil and surface water of the region with several persistent organic pesticides. The total OCPs level
ranged from 0.36–104.50 ng g–1 and 2.63–3.72 μg L–1 in soil and surface water samples, respectively. 相似文献
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采用固相萃取-气相色谱-质谱法(SPE-GC-MS)同时测定水中26种有机氯农药和8种氯苯类化合物,通过选择合适的SPE小柱、优化固相萃取和仪器检测的条件,使该方法在0.050 0 mg/L~1.00 mg/L范围内线性良好。各目标物的方法检出限为0.021μg/L~0.069μg/L,空白水样的加标回收率为36.6%~133%,RSD为0.5%~12.4%。 相似文献
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基于生态风险评价方法对海水淡化和直流冷却两类海水利用工程排放水中的3类典型有机氯农药进行了环境安全性分析。通过实际监测获得有机氯农药在海水利用排放水中的环境浓度;借助美国环境保护署(EPA)颁布的水质基准,获得有机氯农药在海水中的无影响浓度;采用商值法对海水利用排放水中的有机氯农药环境风险进行量化。结果表明:海水利用排放水中七氯和滴滴涕已存在环境风险,其中七氯的污染问题应尤引起重视。 相似文献
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采用固相萃取(SPE)技术,结合气相色谱/质谱(GC-MS)选择离子检测法(SIM)对水样中26种有机氯农药(OCPs)进行提取、净化、浓缩前处理,优选了固相萃取小柱填料及萃取、净化条件,优化了GC-MS的工作参数,建立了地下水中26种有机氯农药的SPE-GC-MS分析方法。针对不同的组分,本法加标回收率为76.422%~112.512%,相对标准偏差为4.905%~15.524%,检出限为0.014~0.089μg/L。该方法操作简单,消耗费用低,分析速度快,具有较高的灵敏度和回收率。 相似文献
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The Contamination Levels of Organochlorine Pesticides in Water and Sediment Samples in Uluabat Lake, Turkey 总被引:3,自引:0,他引:3
The Uluabat Lake is a reservoir of 125 km2 surface area, in the boundaries of Bursa province, Turkey. The results showed that Uluabat Lake was still contaminated by
organochlorine pesticides and their residues despite the existence of bans over a long time. Considerable amounts of organochlorine
pesticides (HCB, p.p′-DDT, p.p′- DDE, α -, β- and γ-BHC, Aldrin, Heptachlor epoxide, Endrin, Endosulfan I and II) were detected in water and sediment samples during one-year
study in this lake. Samples of water and sediment were collected in different regions, (6 sampling point) of the lake between
February 2002 and November 2002.The mean levels of organochlorine pesticides in water and sediments were determined. According
to results, it was found that various environs in Uluabat Lake were contaminated by 11 different organochlorine pesticides.
Residue analyses showed that higher organochlorine pesticides and their residues were generally more accumulated in the sediment
samples. 相似文献