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An efficient, reproducible and rapid fused silica capillary column gas chromatographic method, in splitless mode, for analysing of the three chloroanthracene isomers is described. The method affords efficient separation and good linearity for each isomer in the range of 0.2 -200 μg/ml. The method can also be used in separation and determination of another thirty three aromatic and their halosubstituted compounds. This paper also presents the applications of the method in analysing of complex products mixture from reaction of the selected aromatic compounds with hydrogen chloride on fly ash surface from municipal incinerator. 相似文献
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Two assays were designed to obtain information about the influence of redox potential variations on barium mobility and bioavailability in soil. One assay was undertaken in leaching columns, and the other was conducted in pots cultivated with rice (Oryza sativa) using soil samples collected from the surface of Gleysol in both assays. Three doses of barium (100,300 mg kg−1 and 3000 mg kg−1-soil dry weight) and two redox potential values (oxidizing and reducing) were evaluated. During the incubation period, the redox potential (Eh) was monitored in columns and pots until values of −250 mV were reached. After the incubation period, geochemical partitioning was conducted on the barium using the European Communities Bureau of Reference (BCR) method. Rainfall of 200 mm d−1 was simulated in the columns and in the planting of rice seedlings in the pots. The results of the geochemical partitioning demonstrated that the condition of reduction favors increased barium concentrations in the more labile chemical forms and decreased levels in the chemical forms related to oxides. The highest barium concentrations in leached extracts (3.36 mg L−1) were observed at the highest dose and condition of reduction at approximately five times above the drinking water standard. The high concentrations of barium in the soil did not affect plant dry matter production. The highest levels and accumulation of barium in roots, leaves, and grains of rice were found at the highest dose and condition of reduction. These results demonstrate that reduction leads to solubilization of barium sulfate, thereby favoring greater mobility and bioavailability of this element. 相似文献
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Gomes Brener Felipe Melo Lima de Araújo Caroline Maria Bezerra do Nascimento Bruna Figueiredo Freire Eleonora Maria Pereira de Luna Da Motta Sobrinho Mauricio Alves Carvalho Marilda Nascimento 《Environmental science and pollution research international》2022,29(12):17358-17372
Environmental Science and Pollution Research - In this work, graphene oxide (GO) was synthesized by the modified Hummers method. The nanomaterial was characterized by FTIR and Raman spectroscopy,... 相似文献
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Dulce Buchala Bicca Rodrigues Paulo Tarso Sanches Oliveira Teodorico Alves Sobrinho Eduardo Mario Mendiondo 《Environment, Development and Sustainability》2013,15(4):1037-1048
The Brazilian program of payment for environmental services (PES) is based on ranges of potential erosion decrease (ED) from soil and water conservation proposals estimated from the Universal Soil Loss Equation. Changes in land use and land cover (LULC) result in many alterations of the basin water balance. Therefore, to contribute to the methodological development of Brazilian PES, this paper proposes a quantification of hydrological benefits based on conservation measures. We propose basing the PES program on adding the potential water storage increase (WSI) parameter estimated from the runoff curve number model. Two LULC change scenarios were run considering conservation measures on degraded areas. We found that indicators of ED and WSI were compatible tools for driving the eligibility of soil and water conservation measures. However, the water storage parameter seems to be better at managing the PES mechanism because it is based on water prices and can contribute to appreciation of the efforts performed by the rural producers. The use of the SCS-CN method presents greater feasibility as a tool for the implementation of PES programs in ungauged basins. Thus, an analysis of the success of the innovation proposal of the Brazilian PES program allows inferences to be made about the quantification and financial valuation of hydrological benefits of the potential storage increase and current water price. 相似文献
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da Silva Maryne Patrícia de Souza Ziani Santana Bandeira Cavalcanti Jorge Vinicius Fernandes Lima Fraga Tiago José Marques da Motta Sobrinho Maurício Alves Ghislandi Marcos Gomes 《Environmental science and pollution research international》2021,28(19):23684-23698
Environmental Science and Pollution Research - Multilayer graphene oxide (mGO) was synthesized and functionalized via co-precipitation method to produce magnetic Fe3O4-functionalized multilayer... 相似文献
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de Souza Ziani S. B. Silva Maryne P. Fraga Tiago J. M. Motta Sobrinho Maurício A. 《Environmental science and pollution research international》2021,28(19):23912-23928
Environmental Science and Pollution Research - The present work aims to evaluate the treatment of the effluent from the textile industry via advanced oxidative processes of photo-Fenton assisted by... 相似文献
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水稻杂交后代表观直链淀粉质量分数与蜡质基因(CT)n微卫星多态性的相关性 总被引:2,自引:0,他引:2
以来自2 个水稻杂交组合的后代遗传群体为材料,研究了蜡质基因( Wx) 微卫星标记(CT)n 多态性与稻米表观直链淀粉质量分数( w(AA)) 之间的相关性. 第1 个群体是浙农8010 与嘉育293 的杂交F6 代育种品系,双亲均为籼稻,w(AA) 分别为8 .7% 和25.6 % ,Wx 基因型为分别为(CT)18(CT)18 和(CT)11(CT)11 .另一群体为CM101 与IGRA409 杂交F5 家系,亲本CM101 为一个粳型糯稻,Wx 基因型为(CT)18(CT)18 ;IGRA409 为籼稻,w(AA) = 27.5% ,Wx 基因型为(CT)11(CT)11 .结果发现,在2 个杂交组合的后代群体中,高w(AA) 材料Wx 基因型均为(CT)11(CT)11 ,低w(AA) 及糯稻的均为(CT)18(CT)18 ,中等w(AA) 材料的则为(CT)18(CT)11 的杂合体.统计分析表明,Wx 基因型与w(AA)之间存在显著的相关性,在浙农8010×嘉育293 和CM101 ×IGRA409 两个群体中相关系数分别达0 .9509 和0.9704. 相似文献
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Erica Souto Abreu Lima Talita de Santana Matos Helena Saraiva Koenow Pinheiro Leonardo Durval Duarte Guimarães Daniel Vidal Pérez Nelson Moura Brasil do Amaral Sobrinho 《Environmental monitoring and assessment》2018,190(6):364
The increasing concern regarding the preservation of soil quality suggests the adoption of quality reference values as a first step in environmental monitoring actions. In this context, the objective of this study was to establish soil quality reference values for Al, Zn, Mn, Cd, Fe, Pb, Ni, Cr, and Cu and to correlate several soil properties with the occurrence of these elements in the hillslope region of Rio de Janeiro State. Sixty-two samples were collected at depths of 0–20 and 20–40 cm and analyzed using the USEPA method 3051A. After clustering analysis, the samples were separated into three groups. Classification functions were obtained based on the variables pH - Mg - Fe - Mn, i.e., the variables that were best related to heavy metal content. We determined to establish the quality reference values for the 75th percentile of the three groups. The relief forms of the area, which facilitate the transport of soil fine-particle fractions and accumulation in lowlands, were revealed to be one of most important factors in understanding the distribution of soil heavy metals. 相似文献
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de Oliveira Laís Roberta Galdino dos Santos Filho Derovil Antonio Fraga Tiago José Marques Jucá José Fernando Thomé da Motta Sobrinho Maurício Alves 《Journal of Material Cycles and Waste Management》2021,23(4):1646-1656
Journal of Material Cycles and Waste Management - In this work, food wastes (FWs) and domestic sewage sludge (DSS) were used as raw materials for energy recovery by anaerobic digestion (AD). AD was... 相似文献