BCO分光光度法快速测定含铜三氯化铁蚀刻废液中的铜

采用双环已酮草酰二腙 (简称BCO)光度法 ,对含铜三氯化铁蚀刻废液综合利用过程中铜的快速测定进行了研究。重点对铁基体对于铜测定的干扰情况进行了研究。在选择的最佳分析条件下 ,测定三氯化铁蚀刻废液综合利用过程含铜浓度为 0 4 6g L的还原液时 ,其相对标准偏差和加标回收率分别为 1 0 5 %、99 2 1%、10 0 2 %。本方法简单快速 ,测定 1～ 2个样品仅需 30min。     

乐果对金鱼的急性毒性影响

用改进的寇氏法（karber）测定了乐果对金鱼（Carassius auratus）的急性毒性。急性试验经150mg／L、188．4mg／L、234．4mg／L、291．7mg／L、360mg／L乐果暴露4d，在15％～20％下，24、48、72、96h的L11m值分别为297．17、289．13、259．12、238．67mg／L，其95％置信限分别为284．25～310．67、275．17～303．81、243．33～275．93、223．98～254．33mg／L。     

Characteristics of phosphorus chemistry and its geographical distribution in the Haihe River valley,North China

ＣｈａｒａｃｔｅｒｉｓｔｉｃｓｏｆｐｈｏｓｐｈｏｒｕｓｃｈｅｍｉｓｔｒｙａｎｄｉｔｓｇｅｏｇｒａｐｈｉｃａｌｄｉｓｔｒｉｂｕｔｉｏｎｉｎｔｈｅＨａｉｈｅＲｉｖｅｒｖａｌｌｅｙ，ＮｏｒｔｈＣｈｉｎａＪｉａｎｇＧａｏｍｉｎｇ；ＨｕａｎｇＹｉｎｘｉａｏ；Ｌ...     

Yellow River Valley flood and drought disaster:spatial-temporal distribution predictionand early-warning

ＹｅｌｌｏｗＲｉｖｅｒＶａｌｌｅｙｆｌｏｏｄａｎｄｄｒｏｕｇｈｔｄｉｓａｓｔｅｒ：ｓｐａｔｉａｌ－ｔｅｍｐｏｒａｌｄｉｓｔｒｉｂｕｔｉｏｎｐｒｅｄｉｃｔｉｏｎａｎｄｅａｒｌｙ－ｗａｒｎｉｎｇＧａｏＬｉｎ，ＳｈａＷａｎｙｉｎｇ，ＬｉｕＨｕａｉｑｕａｎ，...     

Normal development in two six-year-old boys born after prenatal diagnosis of trisomy 20 mosaicism

Prenatal diagnosis of trisomy 20 mosaicism was made in two pregnancies by chromosome analysis of cultured amniotic fluid cells. In both cases, the pregnancy continued to term and a healthy male infant was delivered. Regular assessments up to the age of 6-5 years revealed normal physical and intellectual development in both children.     

Duration of vaginal bleeding and trisomy at prenatal diagnosis

In the case-control study of 118 women with autosomal trisomy identified at prenatal diagnosis and their 442 karyotypically normal matched controls, we found that there was no overall association between risk of trisomy and the presence of vaginal bleeding during pregnancy. However, a lengthy duration of bleeding appears to predict increased risk of trisorny.     

Exclusion of citrullinaemia in the first trimester of pregnancy by direct assay of argininosuccinate synthetase in chorionic villi

Citrullinaemia was presumed to be excluded in a fetus at risk by the direct assay of argininosuccinate synthetase in chorionic villi. The diagnosis was confirmed after amniocentesis by normal argininosuccinate synthetase activity in the cultured amniotic fluid cells and by a normal citrulline concentration in the amniotic fluid. The prediction of a normal fetus was confirmed at term by the birth of a non-citrullinaemic boy.