用钛白废酸制备氯化铁和硫酸

采用溶剂萃取与蒸发浓缩相结合的方法综合利用钛白废酸。实验结果表明:向钛白废酸中加入一定量的盐酸,用磷酸三丁酯(TBP)萃取Fe3 ,得到萃合物为HFeCl4.2TBP;在萃取相比(有机相与水相的体积比)与反萃取相比(水相与有机相的体积比)均为1的条件下,用2.53mol/L的TBP对c(Fe3 )=1.023mol/L、c(HCl)=4.53mol/L的试样进行连续5级逆流萃取与反萃取后,得到纯度高达99.88%、总产率达99.4%的氯化铁;萃余液经一次性蒸发浓缩,可得到质量分数80%以上的硫酸。     

用系统生成技术提高会计电算化系统的安全性

会计电算化是管理现代化的重要组成部分 ,会计电算化系统的安全性一直是管理信息系统的难点之一。根据多年实践的经验 ,提出采用系统生成技术改进提高会计电算系统的安全性 ,有助于广大中小企业会计电算化的推广应用。     

极端干湿循环作用下饱和泥浆红黏土的干缩裂隙发育特征

云贵高原红黏土常经历极端干湿循环过程,为研究极端干湿循环作用对红黏土干缩裂隙发育规律的影响,以昆明呈贡地区红黏土饱和泥浆样为研究对象,在室内进行5次干湿循环试验,通过监测红黏土质量和表面干缩裂隙的形成及其演化过程,分析了极端干湿循环作用对红黏土水分蒸发、干缩裂隙的形成及其演化、表面干缩裂隙网络结构形态的影响.结果 表明...     

Testing homogeneity of capture probabilities of animals in a removal experiment

Consider the removal experiment used to estimate population sizes. Statistical methods towards testing the homogeneity of capture probabilities of animals, including a graphical diagnostic and a formal test, are presented and illustrated by real biological examples. Simulation is used to assess the test and compare it with the χ² test.

南黄海6.1级地震及其跟踪预报过程

描述了１９９６年１１月９日南黄海６．１级地震的参数、序列特征、地震构造背景及其跟踪预报过程，并对有关问题进行了讨论     

Relationship between environmental exposure to toluene,xylene and ethylbenzene and the expired breath concentrations for gasoline service workers

This study evaluated the relationship between the breath concentrations of, and personal exposure to, toluene, xylene and ethylbenzene of thirty workers from ten gasoline stations. Personal exposure air samples and workplace samples were collected simultaneously. Each subject provided a sample of exhaled breath after his or her personal exposure air was sampled. Twenty-five personal air, 17 workplace and 30 breath samples were collected in this study. Results indicated that breath concentrations of toluene and xylene were significantly correlated with personal monitoring concentrations. Furthermore, multiple regression analysis showed that exhaled toluene levels were highly influenced by personal toluene concentrations and the amount of personal gasoline sold (r2 = 0.762), while exhaled xylene levels depended on wind speed and personal xylene exposure concentrations (r2 = 0.665). Exhaled ethylbenzene levels were too low to present a relationship between concentrations and personal exposure levels. The exhaled toluene, xylene and ethylbenzene concentrations ranged from 4.3 to 41.8, 0.9 to 13.9, and 0.2 to 6.5 ppb, and the corresponding personal monitoring concentrations ranged from 60.3 to 572.3, 16.4 to 156.6, and 10.7 to 136.6, respectively. The average number of symptoms per person, according to neurotoxic questionnaire 16 (abbreviated as Q16) was 4.1 and six workers showed over six symptoms in Q16. This study suggests that exhaled toluene and xylene levels are suitable for use as biological exposure indices even at the ppb-level of exposure. Gasoline service workers are exposed to high levels of volatile organic compounds (VOCs) and the potential threats to their neurological systems deserve further investigation.     

恐怖袭击风险减缓实例分析

为避免被安全机构监视和追踪 ,恐怖组织常常利用网络结构的优势 ,通过对被动支持者的渗透 ,以突然出现的聚集群方式发动恐怖袭击。军队、警察等传统的反恐工具在试图压制这种多源性恐怖活动时将面临更大挑战。以“东突”问题为例 ,应用物理学的渗透概念模拟特定区域恐怖袭击威胁的形成机理 ,从理论上分析了采取非破坏性手段减缓恐怖袭击风险的可行性。     

城市公共场所人群拥挤踩踏事故分析

城市公共场所人群高度聚集、流动性大,紧急状态时常发生群死群伤的拥挤踩踏事故,造成大量人员伤亡和恶劣的社会影响。笔者首先提出拥挤踩踏事故分析的一般方法,并用群集指数来表征人群高度聚集这一参量;通过对近年来国内外人群拥挤踩踏事故的分析,认为该类事故以人群高度聚集为条件,由公众造成又危害公众,具有诱因众多、发生突然、难以控制等特点;强调事故预防和控制重点是建立事故应急机制,加强人群的管理和疏导等;同时从公共场所的性能优化设计、人群素质和群集密度、人群管理控制以及信息交流等方面分析其事故原因及提出相应对策,对预防此类事故发生,减少群集伤亡有重要意义。     

高层建筑火灾风险的概率模糊综合评价方法

火灾风险评价是减小和控制高层建筑火灾的基本手段。目前 ,高层建筑火灾风险的评价方法很多 ,但是很少有将概率方法与模糊评价方法相结合进行火灾风险评价的。笔者基于对高层建筑火灾风险因素的综合分析 ,建立了高层建筑火灾风险的概率模糊综合评价模型 ,并以具体的工程实例 ,论述了该数学模型在高层建筑火灾风险评价中的应用 ,目的在于为高层建筑火灾风险评价方法的研究提供一种新的尝试 ,为采取合理的火灾防治技术措施在理论上、方法上提供有益的指导。     

48 m环形加热炉系统的事故研究与分析

通过环形加热炉系统的事故类型研究分类与汇总，以及火灾爆炸事故和CO中毒事故的定性定量分析，使现场操作维修人员在安全生产管理中，能够准确地抓住环形加热炉系统事故隐患的关键所在，进而更加科学合理地控制好设备的正常运行，保障安全生产。