Separation of selected PAHs by using high performance capillary electrophoresis with modifiers

The effect of varying SDS concentration in a micellar electrokinetic capillary chromatographic system (MECC) is investigated. In addition, the introduction of -cyclodextrin as modifier to the electrophoretic medium, containing SDS and a phosphate-borate buffer, is shown to give satisfactory separation of the seven selected PAHs. The separation efficiency is increased with the addition of -cyclodextrin.     

水中Mg~(2+)的测试管快速测定

研制了一种测定水中Mg2 + 的测试管 ,测定范围为 0 .5mg/L～ 2 .0mg/L。该测试管适用于现场应急监测 ,具有快速、简便、抗干扰能力强和价格低廉等特点     

连续采样与五日法采样效果及费用的对比分析

通过对连续采样与五日法采样五种方法监测结果及所需费用的比较，得出连续采样方法监测结果更具有代表性，合理性，一次性投资大，但运行费用并不高的结论。     

Development of an ombrotrophic peat bog (low ash) reference material for the determination of elemental concentrations

Given the increasing interest in using peat bogs as archives of atmospheric metal deposition, the lack of validated sample preparation methods and suitable certified reference materials has hindered not only the quality assurance of the generated analytical data but also the interpretation and comparison of peat core metal profiles from different laboratories in the international community. Reference materials play an important role in the evaluation of the accuracy of analytical results and are essential parts of good laboratory practice. An ombrotrophic peat bog reference material has been developed by 14 laboratories from nine countries in an inter-laboratory comparison between February and October 2002. The material has been characterised for both acid-extractable and total concentrations of a range of elements, including Al, As, Ca, Cd, Cr, Cu, Fe, Hg, Mg, Mn, Na, Ni, P, Pb, Ti, V and Zn. The steps involved in the production of the reference material (i.e. collection and preparation, homogeneity and stability studies, and certification) are described in detail.     

火焰原子吸收分光光度法测定鱼内脏及河流底泥中的铜

采用火焰原子吸收分光光度法测定鱼内脏及河流底泥中的铜。鱼内脏经组织捣碎机捣成匀浆后，加硝酸消解；底泥则经氢氟酸和高氯酸消化。该方法具有灵敏度高，精密度和回收率较好等特点。     

离子交换树脂光度法测定微量铁的研究

研究了以阳离子交换树脂为显色载体，利用直接吸附在树脂上有色络合物－Fe(II)邻二氮菲的吸光度，借以检测水和火腿肠中铁的新方法，本法具有比原子吸收法更高的灵敏度，稳定性和选择性，并对成络及树脂吸附条件作了较详细研究。     

粗苯污染事故应急处理

针对一次苯泄漏事故的应急处理过程、方法进行论述与总结，并分析了事故现场周围地表、地下水中苯污染浓度的变化情况，提出了该类事故的应急措施，以此作为处理同类事故的参考和依据。     

乌鲁木齐市汽车尾气污染状况调查

对乌鲁木齐市主要街道受汽车尾气污染的调查和综合分析得到CO、NOx、HC的污染规律,主要街道路中心空气中CO、NOx日均值已超出国家大气环境质量二级标准,市区主要街道的人行道空气中NOx含量已超出二级标准,Ⅱ、Ⅲ类道路人行道空气中CO含量已超标;在三类街道中,Ⅰ类街道车流量最大,Ⅱ类次之,Ⅲ类最少,而汽车排放尾气对街道空气污染状况为Ⅲ类最重、Ⅱ类次之、Ⅰ类最轻。     

中国北方干旱地区沙尘矿物特征研究

为了开展对我国沙暴传输规律的研究,了解我国北方干旱地区沙尘矿物特征有重要意义。本文对我国新疆塔克拉玛干沙漠区,内蒙腾格里沙漠区,贺兰山及银川等处的沙尘样品用X射线粉末衍射法进行矿物分析鉴定,并用原子吸收法作了特征元素的分析对比,根据矿物的X射线粉末衍射结果,结合元素分析,对沙漠源区及其以东地区沙尘矿物特征作了比较,判析了两个源区的矿物组成,讨论了它们的传输过程。     

唐山市空气中SO2与TSP污染状况分析

分析了唐山市从1988年至1992年大气中SO2和TSP的污染状况和变化规律，取得对该市环境管理的科学依据。