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791.
Najam A. Shakil Alka Pandey Manish K. Singh Jitendra Kumar Satish K. Awasthi Pankaj 《Journal of environmental science and health. Part. B》2013,48(2):108-115
A new series of 1, 3-Benzoxazines were synthesized, characterized (1H NMR and 13C NMR) and evaluated for their pesticidal activity. Six new 3-alkyl-3, 4-dihydro-4-methyl-2H-1, 3-benzoxazines (1-6) were prepared by hydroxymethylation of secondary amines with formaldehyde in 65–68% yields. These compounds were screened for there IGR activity against Spodoptera litura and for antifungal fungal activity in vitro against Sclerotium rolfsii ITCC 6181 by poisoned food technique. Insect Growth Regulatory (IGR) activity against Spodoptera litura showed that compound 3-Nonyl-3,4-dihydro-4-methyl-2H-1,3-benzoxazines was most effective as IGR with larval GI50 of 1.863 μ g/Insect. Compounds 3-Octyl-3,4-dihydro-4-methyl-2H-1,3-benzoxazines and 3-Decyl-3,4-dihydro-4-methyl-2H-1,3-benzoxazines were effective IGRs. Antifungal screening revealed that compound 3-Dodecyl-3, 4-dihydro-4-methyl-2H-1,3-benzoxazines, was highly effective against Sclerotium rolfsii with LC50 value 31.7 mg L?1 comparable with commercial fungicide Hexaconazole (LC50 1.27 mg L?1). Also compounds 3-Nonyl-3, 4-dihydro-4-methyl-2H-1,3-benzoxazines and 3-Decyl-3,4-dihydro-4-methyl-2H-1,3-benzoxazines displayed promising fungitoxicity. The results described in this paper are promising and provides new array of synthetic chemicals to be utilized as pesticides. 相似文献
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Atmospheric deposition studies of heavy metals in Arctic by comparative analysis of lichens and cryoconite 总被引:1,自引:0,他引:1
Shiv Mohan Singh Jagdev Sharma Puja Gawas-Sakhalkar Ajay K. Upadhyay Simantini Naik Shailesh M. Pedneker Rasik Ravindra 《Environmental monitoring and assessment》2013,185(2):1367-1376
Lichens and cryoconite (rounded or granular, brownish-black debris occurring in holes on the glacier surface) from Ny-Ålesund were used for understanding the elemental deposition pattern in the area. Lichen samples collected from low-lying coastal region and cryoconite samples from high altitudinal glacier area were processed and analysed for elements such as aluminium (Al), arsenic (As), cadmium (Cd), cobalt (Co), chromium (Cr), cesium (Cs), copper (Cu), iron (Fe), manganese (Mn), nickel (Ni), lead (Pb), vanadium (V) and zinc (Zn) through inductively coupled plasma mass spectrometry. Results showed that heavy metals, Al and Fe, are present in high concentration in the cryoconite samples. Al was also present in high amounts in seven of the eight lichen samples studied. The general scheme of elements in the decreasing order of their concentrations for most of the cryoconite samples was Al?>?Fe?>?Mn?>?Zn?>?V?>?Pb?>?Cr?>?Ni?>?Cu?>?Co?>?As?>?Cs?>?Cd while that for the lichen samples was Al?>?Fe?>?Zn?>?Mn?>?Pb?>?Cu?>?Cs?>?Cr?>?Ni?>?V?>?Co?>?As?>?Cd. Similarity in trends in the two sample types confirms that the environment indeed contains these elements in that order of concentration which overtime got accumulated in the samples. Overall comparison showed most elements to be present in high concentrations in the cryoconite samples as compared to the lichen samples. Within the lichens, elemental accumulation data suggests that the low-lying site (L-2) from where Cladonia mediterranea sample was collected was the most polluted accumulating a number of elements at high concentrations. The probable reasons for such deposition patterns in the region could be natural (crustal contribution and sea salt spray) and anthropogenic (local and long-distance transmission of dust particles). In the future, this data can form a baseline for monitoring quantum of atmospheric heavy metal deposition in lichens and cryoconite of Svalbard, Arctic. 相似文献
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The treatment of groundwater contaminated with low concentrations of methyl tertiary butyl ether (MTBE) is of nationwide concern. Many treatment techniques include removing MTBE vapors from groundwater, resulting in airstreams that require treatment. One method used for air‐phase MTBE treatment is biofiltration. In a biofilter, the vapors pass through a reactor that contains MTBE‐biodegrading organisms attached to a porous media. This article reports the results of a biofiltration study to treat air contaminated with MTBE at concentrations of 0.2 to 0.33 mg/l, concentrations frequently encountered in the field. The results indicate that MTBE removal at these low concentrations is not as efficient as removals seen at higher concentrations. Activated carbon was shown to be a superior biofiltration medium, compared with media that do not adsorb MTBE vapors. Activated carbon was especially helpful in treatment shock loads of MTBE. © 2002 Wiley Periodicals, Inc. 相似文献
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