A sensitive monoclonal antibody-based enzyme-linked immunosorbent assay for chlorpyrifos residue determination in Chinese agricultural samples

A monoclonal antibody-based competitive antibody-coated enzyme-linked immunosorbent assay (ELISA) was developed and optimized for determining chlorpyrifos residue in agricultural products. The IC₅₀ and IC₁₀ of this ELISA were 3.3 ng/mL and 0.1 ng/mL respectively. The average recoveries in six agricultural products were between 79.5% and 118.0%, with the intra-assay coefficient of variation being less than 8 %. The limit of detection for all tested products was 30 ng/g. To the best of our knowledge, this assay has the best specificity among all the published research on ELISAs for chlorpyrifos.     

空心壳聚糖微球对二甲酚橙的吸附性能研究

以生物可降解的壳聚糖为原料,采用反相悬浮交联法制备了具有空壳结构的壳聚糖微球,通过控制反应条件得到单分散性的微米级微球.通过分光光度法探讨了溶液初始pH、吸附时间、二甲酚橙初始浓度、壳聚糖微球用量及其直径对壳聚糖微球吸附二甲酚橙的影响.结果表明,常温下壳聚糖微球对二甲酚橙的最佳吸附条件为:溶液初始pH为5,吸附时间为2.0 h,二甲酚橙初始质量浓度为32 mg/L,壳聚糖微球用量为0.3 g/L(以每升二甲酚橙溶液计),壳聚糖微球直径为74 靘;在此最佳吸附条件下,采用分光光度法对二甲酚橙模拟废水进行测定,相应的回收率误差均在-1%～1%.     

Distribution and variation of mercury in frozen soils of a high-altitude permafrost region on the northeastern margin of the Tibetan Plateau

Environmental Science and Pollution Research - The Tibetan Plateau (TP) is home to the largest permafrost bodies at low- and mid-latitudes, yet little is known about the distribution and variation...     

Energy-Saving Effect Calculation and Implementation Strategy Study on the Industrial Structure Adjustment in Western China

The western region is an important strategic base of energy in China. The average per capita possession of fossil energy in the west is twice that in China. On the basis of the analysis of the mechanism how industrial structure adjustment affects energy consumption per unit of gross domestic product (GDP), the energy input-output table of western China was designed and compiled. Combining multiobjective planning techniques, setting energy-saving, economic growth, and laborer's income growth as the goals, setting basic input-output relations, production capacity, and labor as the constraints, the multiobjective optimization model of western energy input-output was constructed. The results of industrial structure optimization of western China show that: with technology and product price remaining unchanged, the adjustment of the industrial structure can reduce energy consumption per unit GDP by 2.7%, at the same time ensuring the average annual increase of GDP and laborer's income of western region in excess of 8%. It indicates that industrial structure adjustment is an effective method in accomplishing the aim of energy saving. Finally, policy suggestions from four angles, such as industrial chain and financial policies, were put forward.     

Innovative cleaner production for steel phosphorization using Zn–Mn phosphating solution

Phosphating prior to coating for steel is usually needed. In this paper, an innovative cleaner production has been developed for steel surface treatment using Zn–Mn phosphating solution in which there was no nitrite. The mass of the Zn–Mn layer deposited in this new process was about 1.1 g m^?2 when the temperature ranged from 3 to 35 °C. The corrosion time for the color phosphating layer in the copper sulfate spot test was in the range of 72–145 s. Adhesion test showed that the coating layers achieved a higher adhesion load than those produced by conventional methods. Washing using water was not necessary in this cleaner phosphorization, which usually follows phosphorization in traditional processes of steel phosphorization. Consequently, wastewater discharge was reduced greatly.     

实验室检测/校准方法的确认研究

结合实验室方法确认工作中的经验,从方法确认的内容、过程、结果以及记录的形成等方面,阐述了实验室方法确认工作有效开展的保障措施。     

综合防治棉铃虫的区域性技术体系研究

研究改进了棉铃虫中期预报方法；提出“一代监测、二代保顶、三代保蕾、四代保铃”为主的防治策略；研究制定适用于不同世代、不同水肥条件的科学防治指标，协调应用多种配套措施保护、利用自然天敌控害，系统监测和治理棉铃虫抗药性；利用棉花种质资源和品种的抗病、抗虫性；诱杀成虫；组建大面积综防技术体系。在１９９２～１９９５年棉铃虫猩獗发生的情况下，于河南省新乡县棉花病虫害综防示范区大面积实施后，有效控制了棉铃虫危害。     

天津市城市污水自由水面构筑物湿地处理系统中污水氮去除规律的研究

天津市城市污水自由水面构筑物湿地处理系统中，污水氮的去除效果受到场地坡长，水力负荷，停留时间，温度，预处理水质等因素的影响，本文根据试验场地实际运行的数据，讨论了上述因素与污水氮去除率的关系，结果表明，系统对污水氮的去除率，与坡长在一定范围内呈正线性相关关系，与水力负荷呈负的线性相关关系，停留时间为７８ｈ时除氧效果最佳，温度对氮去除率的影响随着季节变化表现出来，没有直接规律性，预处理水质对系统的除     

裂解气脱硫新趋势

在回顾现有裂解气脱硫工艺的基础上，介绍了近年来国内外在该领域的研究和应用中所取得的进展及未来的发展趋势。