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111.
Leila Hajiaghababaei Babak Ghasemi Alireza Badiei Hassan Goldooz Mohammad Reza Ganjali Ghodsi Mohammadi Ziarani 《环境科学学报(英文版)》2012,24(7):1347-1354
A rapid method for the extraction and monitoring of nanogram level of Pb2+ and Cu2+ ions using uniform silanized mesopor (SBA-15) functionalized with aminobenzenesulfonamide groups and flame atomic absorption spectrometry (FAAS) is presented. Aminobenzenesulfonamide functionalized SBA-15 was synthesized according to procedure in the literature and the presence of organic groups in the silica framework was demonstrated by FT-IR spectra. The functionalized product showed the BET surface area 110 m2/g and pore diameter 5.1 nm, based on adsorption-desorption of N2 at 77 K. The effect of several variables such as (amount of adsorbent, stirring time, pH and presence of other ions in the medium) has been studied. Lead and copper were completely extracted at pH greater than 3 after stirring for 10 min. The maximum capacity of the adsorbent was found to be 191.3 ± 1.4 and 155.0 ± 1.0 μg of lead and copper ions/mg functionalized SBA-15, respectively. The preconcentration factor of the method was found to be 200. The detection limit of the technique was 3.4 and 0.4 ng/mL for Pb2+ and Cu2+, respectively. The applications of this methodology for real samples were examined by various water type, black tea and pepper samples. 相似文献
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Biological samples are extracted with n-hexane/acetone (60:40) and 1 mL of the concentrated extract is eluted through a pasteur pipette column prepacked with alumina (0.3 g) and silicic acid (0.25 g) with 10 mL n-hexane (containing 4% acetone). The fat and other co-extractives are retained by the column and clear eluate is directly injected on a GLC column for determination on electron capture detector. A comparison of the Pasteur pipette cleanup with the modified method of Cole et al. (1967) on 41 samples of fish, One Step Method, (Ahmad and Marolt (1986] on 86 samples of fish and Maunder et al. (1964) on 10 type of wildlife (100 samples) was made. The Pasteur pipette method gives results which are significantly higher (p greater than 0.5) than the other methods except the One step method. The Pasteur pipette method has a detection limit of 0.01 microgram/g for DDT and its metabolites. 相似文献
114.
Used lubricating oil recycling using hydrocarbon solvents 总被引:1,自引:0,他引:1
A solvent extraction process using new hydrocarbon solvents was employed to treat used lubricant oil. The solvents used were liquefied petroleum gas (LPG) condensate and stabilized condensate. A demulsifier was used to enhance the treatment process. The extraction process using stabilized condensate demonstrated characteristics that make it competitive with existing used oil treatment technologies. The process is able to reduce the asphaltene content of the treated lubricating oil to 0.106% (w/w), the ash content to 0.108%, and the carbon residue to 0.315% with very low levels of contaminant metals. The overall yield of oil is 79%. The treated used oil can be recycled as base lubricating oil. The major disadvantage of this work is the high temperature of solvent recovery. Experimental work and results are presented in detail. 相似文献
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Ansari Faiz Ahmad Guldhe Abhishek Gupta Sanjay Kumar Rawat Ismail Bux Faizal 《Environmental science and pollution research international》2021,28(32):43234-43257
Environmental Science and Pollution Research - The aquaculture industry is an efficient edible protein producer and grows faster than any other food sector. Therefore, it requires enormous amounts... 相似文献
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Ebrahimzade Hossein Khayati Gholam Reza Schaffie Mahin 《Journal of Material Cycles and Waste Management》2021,23(6):2218-2231
Journal of Material Cycles and Waste Management - Modeling of leaching process as a function of operational variables can specify an accurate perspective in the forecasting of valuable... 相似文献
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Farooq Muhammad Asim Aquib Md Khan Daulat Haleem Ghayas Sana Ahsan Anam Ijaz Muhammad Banerjee Parikshit Khan Maqsood Ahmed Ahmad Muhammad Masood Wang Bo 《Environmental Chemistry Letters》2019,17(4):1565-1583
Environmental Chemistry Letters - Research has recently focused on combinational therapy using nanocarriers to overcome the obstacles associated with conventional therapy of lung cancer. The... 相似文献