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141.
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Cécile Courdier John Boudjarane Valérie Malan Christine Muti Brian Sperelakis-Beedham Sylvie Odent Sylvie Jaillard Chloé Quelin Cédric Le Caignec Olivier Patat Charlotte Dubucs Sophie Julia Caroline Schluth-Bolard Carole Goumy Sylvia Redon Jean-Baptiste Gaillard Minh Tuan Huynh Céline Dupont Anne-Claude Tabet Guillaume Cogan François Vialard Rodolphe Dard Guillaume Jedraszak Florence Jobic Mathilde Lefebvre Geneviève Quenum Saori Inai Mélanie Rama Fanny Sauvestre Frédéric Coatleven Julie Thomas Caroline Rooryck 《黑龙江环境通报》2023,43(6):734-745
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Solid phase microextraction (SPME) as an effective means to isolate degradation products in polymers 总被引:2,自引:0,他引:2
Minna Hakkarainen Ann- Christine Albertsson Sigbritt Karlsson 《Journal of Polymers and the Environment》1997,5(2):67-73
A new sample preparation technique, solid phase microextraction (SPME), was compared with direct headspace-GC-MS with respect
to the type and amount of identified compounds. Three types of LDPE films containing photosensitising additives according
to the Scott-Gilead patents and pure LDPE were used as model substances. The polyethylene films were thermally aged at 80‡C
after the induction period was surpassed by subjecting the materials to 100 h of UV radiation. The new SPME method was developed
using nonpolar poly(dimethylsiloxane) and polar carbowax fibers to extract the low molecular weight products formed in the
polyethylene films during aging. Many more products were identified after SPME followed by GC-MS than after direct headspace-GC-MS
of the samples. The SPME method allowed the identification of homologous series of carboxylic acids, ketones, and furanones,
while direct headspace-GC-MS identified only a few carboxylic acids (C1-C6) and small amounts of some ketones and furanones.
In general, SPME was more effective in extracting less volatile products, and in particular, the polar carbowax fiber identified
also C7-C12 carboxylic acids and 4-oxopentanoic acid. By SEC and FTIR we confirmed that the number and amount of former degradation
products correlated well with the decrease in molecular weights and the amount of formed carbonyl compounds. 相似文献
146.
Stefaniak AB Hoover MD Day GA Dickerson RM Peterson EJ Kent MS Schuler CR Breysse PN Scripsick RC 《Journal of environmental monitoring : JEM》2004,6(6):523-532
Little is known about the physicochemical properties of beryllium aerosols associated with increased risk of beryllium sensitization and chronic beryllium disease (CBD). Such information is needed to evaluate whether airborne mass of beryllium is the appropriate metric of exposure or alternatively to provide a scientific basis for using information on particle size, surface area, and chemistry to support an improved exposure limit based on bioavailability through the inhalation and dermal routes of exposure. Thus, we used a suite of analytical techniques to characterize aerodynamically size-fractionated beryllium particles and powders that have been associated in epidemiological studies with higher prevalence of CBD. Aerosol particles were sampled from the ventilation systems of production lines for powders of beryllium metal and beryllium oxide and for ingots of copper-beryllium alloy. End product powders from the metal and oxide production lines were also collected.Particles released during production of beryllium metal were found to be complex, having heterogeneous composition, including reactive species such as fluorine. Powders from beryllium metal production were of high purity with only a minor component of beryllium oxide. Both particles and powders from oxide production were high-purity oxide. Particles released during production of copper-beryllium alloy were heterogeneous, being predominantly copper oxides. Thus, all particles and powders contain at least some beryllium in the form of beryllium oxide.These data justify efforts to thoroughly characterize beryllium aerosol properties when performing exposure assessments. The data also suggest that differences in particle chemical composition, size, number, and surface area may influence bioavailability of beryllium and contribute to risk of CBD. However, a scientific basis does not yet exist to replace mass as the current metric of exposure. 相似文献
147.
Willets (Catoptrophorus semipalmatus) were collected in June and August 1986 at the outlets of two agricultural drainages into the Lower Laguna Madre of South Texas and at two other Texas coastal sites. Mean liver concentration of arsenic was higher in August than June. Over 20% of the livers had arsenic concentrations elevated above a suggested background level of 5.0 ppm dry weight (DW), but concentrations (maximum 15 ppm) were below those associated with acute toxicity. Selenium concentration in livers varied from 2.3 to 8.3 ppm DW for all locations and represented background levels. Mercury concentrations in livers for all locations (means = 2.0 to 3.4, maximum 17 ppm DW) were below those associated with avian mortality and similar to levels found in other estuarine/marine birds. DDE in carcasses was higher in adults (mean = 1.0 ppm wet weight) than juveniles (0.2 ppm), and higher in August (1.0 ppm) than June (0.5 ppm); however, DDE concentrations were generally at background levels. Based on brain cholinesterase activity, willets were not recently exposed to organophosphate pesticides. 相似文献
148.
Marwan A. Hassan Dan L. Hogan Stephen A. Bird Christine L. May Takashi Gomi David Campbell 《Journal of the American Water Resources Association》2005,41(4):899-919
This paper synthesizes information on the spatial and temporal dynamics of wood in small streams in the Pacific Northwest region of North America. The literature on this topic is somewhat confused due to a lack of an accepted definition of what constitutes “small” streams and what is the relative size of woody debris contained within the channel. This paper presents a matrix that defines woody debris relative to channel size and then discusses the components of a wood budget. Headwater streams are in close proximity to wood sources and, in steeplands, are often tightly constrained by steep hillslopes. Special consideration is given to ecosystem characteristics and to management practices that affect the wood dynamics in this context. Knowledge gaps and uncertainties that can be used to guide future research are identified. Very little is currently known about the role of mass wasting in wood recruitment and storage relative to other processes, such as bank erosion and mortality, in larger streams. Further, very little work has addressed the relative importance of different wood depletion processes, especially those associated with wood transport. The effect of other ecosystem variables on wood dynamics locally across a watershed (from valley bottom to mountaintop) and regionally across the landscape (from maritime to continental climates) is not addressed. Finally, the scientific community has only begun to deal with the effects of management practices on wood quantity, structure, and movement in small streams. 相似文献
149.
Previous studies imply that individuals with an external locus of control (LOC) are less likely to be committed to their organizations. More recent work on organizational commitment has suggested that commitment is not a unidimensional construct and can take several forms (e.g., affective and continuance). Using a sample of 232 employees of a Canadian governmental agency, we examined the relations between LOC and two different forms of organizational commitment that have been found to have different antecedents and consequences. We found that internal LOC was associated with affective commitment and external LOC was associated with continuance commitment. Implications for research and practice are discussed. Copyright © 1999 John Wiley & Sons, Ltd. 相似文献
150.
Addressing challenges for future strategic‐level emergency management: reframing,networking, and capacity‐building 下载免费PDF全文
The mounting frequency and intensity of natural hazards, alongside growing interdependencies between social‐technical and ecological systems, are placing increased pressure on emergency management. This is particularly true at the strategic level of emergency management, which involves planning for and managing non‐routine, high‐consequence events. Drawing on the literature, a survey, and interviews and workshops with Australia's senior emergency managers, this paper presents an analysis of five core challenges that these pressures are creating for strategic‐level emergency management. It argues that emphasising ‘emergency management’ as a primary adaptation strategy is a retrograde step that ignores the importance of addressing socio‐political drivers of vulnerabilities. Three key suggestions are presented that could assist the country's strategic‐level emergency management in tackling these challenges: (i) reframe emergency management as a component of disaster risk reduction rather than them being one and the same; (ii) adopt a network governance approach; and (iii) further develop the capacities of strategic‐level emergency managers. 相似文献