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211.
Determination of selected neonicotinoid insecticides by liquid chromatography with thermal lens spectrometric detection 总被引:1,自引:0,他引:1
Valéria Guzsvány Azamela Madžgalj Polonca Trebše Ferenc Gaál Mladen Franko 《Environmental Chemistry Letters》2007,5(4):203-208
We studied the analysis of trace amounts of neonicotinoid insecticides by liquid chromatography coupled with a thermal lens
spectrometric detector (TLS). This multi-residue analysis method is based on the reversed phase separation on C18 column, isocratic elution and collinear dual beam TLS detection. The insecticides thiamethoxam, imidacloprid, acetamiprid
and thiacloprid were detected with retention times of 4.4, 5.7, 6.5 and 8.5 min and limits of quantifications of 50, 89, 10,
and 25 μg/L, respectively. The retention times agreed well with those obtained by the same chromatographic method but using
a diode-array detector (DAD). The limits of quantifications for imidacloprid were identical in both techniques. However, the
limits of quantifications for thiamethoxam, acetamiprid and thiacloprid were up to 8.5 times lower using the TLS detector
compared to the diode-array detector. The applicability of the developed procedure was tested on spiked river water and potato
samples. 相似文献
212.
介绍了冲压上常见的大型覆盖件的冲压工艺方案的确定过程 ,并以S0 1农用皮卡车“前地板”为例 ,针对此件外形复杂 ,成形深度大 ,模具加工周期大 ,成本高等问题 ,进行了详细的冲压工艺分析 ,确定了合理的冲压工序 ,且着重介绍了修边冲孔模具的设计要点及简化模具加工工艺 ,降低模具成本 ,缩短制模周期等措施 相似文献
213.
厌氧颗粒污泥反应器修复模拟受PCP污染地表水的性能研究 总被引:2,自引:1,他引:2
研究了用于修复模拟受PCP污染地表水的厌氧颗粒污泥反应器降解PCP活性的维持条件和修复性能.结果表明,降解PCP活性可通过连续提供电子供体和选择压力来维持,操作条件为COD进水/PCP进水>30,此时反应器具有稳定的PCP去除和产甲烷性能;颗粒污泥反应器修复受PCP污染地表水的性能与过程稳定性受电子供体类型、数量的影响.当COD/PCP>150—200,HRT为05d时,含PCP1291mg/L的模拟受污地表水经厌氧反应器修复后,其PCP浓度可低于1PPb,生物毒性明显降低. 相似文献
214.
Mrcia Gabriel Genesio Mario da Rosa Arci Dirceu Wastowski Jefferson Alves da Costa Fernanda Volpatto 《环境质量管理》2019,29(2):149-154
Separation of water for reuse is essential in an effluent treatment system, especially in activities with high water consumption, such as a pig production system. The objective of this work was to evaluate the efficiency of Tanfloc SG® coagulant tannin/organic flocculant used to treat effluent generated during the intensive rearing of swine. For the evaluation, laboratory and in situ tests (field test) were performed. The laboratory tests were performed to define the concentration (1 and 16%), dosage (0, 0.1, 0.2, 0.3, 0.4, 0.5, 1.0, 2.0, 4.0, 8.0, and 16.0 milliliters of the solution), and time (24, 48, 72, and 96 hours) of coagulation/flocculation treatment of the solid portion of the effluent. The parameters pH, turbidity, oxidation reduction potential, dissolved oxygen, and electroconductivity (in microsiemens per centimeter) were evaluated using a multiparameter probe and the parameters ammonia (NH3), nitrate (NO3), and nitrite (NO2) in the laboratory, in relation to the coagulation/flocculation time of the solid part of the effluent. The use of tannin as a coagulant/flocculant of plant origin in the treatment of swine effluents was effective in reducing turbidity and concentrations of ammonia, nitrite, and nitrate, and it allowed separation of the solid–liquid phase in approximately 68% as liquid phase. 相似文献
215.
Lucas Veiga Avila Joo Serafim Tusi da Silveira Emitrio da Rosa Neto Daniel Knebel Baggio 《环境质量管理》2019,29(2):129-137
Many universities around the world have served as active centers for research on climate change. However, there are several barriers to their activities, stemming from the nature of research, resources, and the structure of institutions. This document provides an overview of barriers, potential factors, and activities to develop and implement sustainable energy processes in public higher education institutions (HEIs) in Brazil. The research was conducted from March to April of 2018 with representatives of HEIs (rectors or prorectors of research). A total of 63 invitations to respond to the Survey‐monkey survey were emailed, and responses were received from 32 universities. The research concludes by proposing measures that can be taken to make the issue of climate change more present and effective in university research and teaching activities. This includes changes in research, information dissemination, and teaching approaches to better support actions to address climate change. In Brazil, there are many potentialities in terms of natural resources, but actions for implementation are still incipient. Further efforts and investment in research and development will be required. 相似文献
216.
Zeban Shah Renato C. Veses Julio C. P. Vaghetti Vanessa D. A. Amorim Rosangela da Silva 《International Journal of Green Energy》2019,16(4):350-360
The Bio-oil was produced from the pyrolysis of agricultural wastes (Eucalyptus sawdust) and discarded soybean frying oil. The temperature of the pyrolysis system was initiated at 28°C and increased to 850°C. Atmospheric distillation of crude bio-oil was performed and a fraction at a temperature range 160–240°C (pyrolysis oil) was separated and subjected to GC-MS, 1H-NMR, TGA and FTIR analysis to identify the different properties and compounds present in pyrolysis oil. It was noticed that there was an abundance of oxygen and nitrogen containing compounds as well as other reactive species in pyrolysis oil. To reduce the amount of these species, the pyrolysis oil was subjected to hydrogenation in the presence of NiMo as a catalyst. After hydrogenation, the atmospheric distillation of hydrogenated bio-oil was performed and another fraction at temperature range 160–240°C (hydrogenated bio-oil) was separated and analyzed by the same techniques. It was noticed that during hydrogenation, more than 60% oxygenated and other reactive species were converted into hydrocarbons. Hydrogenated bio-oil showed very similar physico-chemical properties such as distillation curve, density, viscosity, freezing point, flash point, the presence of hydrocarbons and enthalpy of combustion as aviation kerosene also known as QAV-1. 相似文献
217.
Miagostovich Marize Pereira Rocha Mônica Simões dos Reis Fabiane Bertoni Sampaio Marcelo Santos de Saldanha da Gama Gracie Carrijo Renata Malta Fabio Correia Rodrigues Janaína Genuino Amanda Ribeiro da Silva Assis Matheus Fumian Tulio Machado Barrocas Paulo Rubens Guimarães 《Food and environmental virology》2020,12(2):130-136
Food and Environmental Virology - The availability of drinking water is one of the main determinants of quality of life, disease prevention and the promotion of health. Viruses are important agents... 相似文献
218.
Juliano Gonçalves Pereira Vanessa Mendonça Soares Fernanda Gil de Souza Leonardo Ereno Tadielo Emanoelli Aparecida Rodrigues dos Santos Mário Celso Sperotto Brum Andreia Henzel Eduarda Hallal Duval Fernando Rosado Spilki Wladimir Padilha da Silva 《Food and environmental virology》2018,10(4):365-372
The aim of this study was to investigate hepatitis A virus (HAV), hepatitis E (HEV), and rotavirus (RV) in fresh and processed meat traded on the border of Brazil with Argentina and Uruguay. In total, 159 samples of raw and processed foods of animal origin were collected in Paso de los Libres, Argentina (n?=?53 raw meat, n?=?24 processed meat) and Rivera, Uruguay (n?=?55 raw meat, n?=?18 processed meat), or were seized by the Brazilian International Agricultural Surveillance System—VIGIAGRO (Brazil–Argentina border) (n?=?8 raw meat, n?=?1 bush meat). All samples were tested for the presence of HAV, HEV, and RV genomes. HAV genes were detected in 18.23% of samples and RV genes in 23.89%. No HEV-positive samples were detected. HAV was also detected in two of the VIGIAGRO samples. Processed meats from Argentina and Uruguay had a higher rate of HAV and RV than raw meat (P?>?0.05). The median HAV in the Argentinian and Uruguayan samples was 6.9?×?104 and 3.5?×?103 copies/g, respectively. The presence of RV viral genes in raw meats from Argentina was significant, and this was not observed in processed meats. The presence of HAV and RV genes in a significant portion of products from Argentina and Uruguay is a potential source of human infection. This also indicates precarious conditions of acquisition, processing, and manipulation, which could be improved by improved regulation of food across borders. 相似文献
219.
Georg Lockemann G. Masing R. Schwarz K. Andrée S. Hollmann 《Die Naturwissenschaften》1953,40(14):395-396
220.
Yuping Zhang Yu´e Wu Anming Yang Jun Wang Kankan Zhang Deyu Hu 《Environmental monitoring and assessment》2017,189(5):226
A total of 54 soil and 54 potato samples have been collected from Weining County to evaluate the accumulation of cadmium in potatoes. The concentrations of the total Cd and the available Cd in the soil samples have been detected. The total concentrations of Cd were from 0.41 to 10.0 mg/kg with an average value of 2.60 mg/kg in soil. The concentrations of available Cd in the soil were 0.07 to 3.47 mg/kg with an average value of 0.59 mg/kg. The concentration of the available Cd showed a good linear positive correlation with the total Cd content in the soil. For the 54 potato samples, the Cd concentrations were from 0.023 to 0.18 mg/kg with an average value 0.083 mg/kg (fresh weight).The bioconcentration factor (BCF) values of Cd in potatoes, based on dry weight, were from 0.02 to 0.96 with an average value 0.24. The uptake of cadmium by plants is dependent on various soil and environmental factors. A regression model to predict the concentration of cadmium in Weining potatoes based on soil properties and elevation was developed. The results showed the elevation and the soil pH played an important role and had a negative influence on the uptake of Cd by potato in Weining County. The mean intake of Cd by adults through consumption of potato from Weining would be 5.9 μg/day, and it is well below the provisionally tolerable daily intake for Cd (70 μg/day). 相似文献