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11.
Ajaz‐ul Haque Irene Weisgerber Dimitris Kotzias Werner Klein Friedhelm Korte 《Journal of environmental science and health. Part. B》2013,48(3):211-223
Abstract The urea herbicide buturon (N‐[p‐chlorophenyl] ‐N’ ‐methyl‐N’ ‐isobutinyl‐urea), 14C‐labeled, was sprayed on winter wheat as an aqueous formulation (2.98 kg/ha) under outdoor conditions. Upon harvest (three months after application), a total of 49. 2% of the applied radiocarbon was recovered: 2.0% in the plants, 46.9% in the soil, and 0.3% in the leaching water (depth > 50 cm); less than 0.1% was in the grains (0.464 ppm). Only about half of the radioactivity present in plants could be recovered under mild extraction conditions; about half of this was unchanged buturon. In straw and husk extracts, the following metabolites were identified by gaschromatography/mass spectrometry: N‐(p‐chlorophenyl)‐N‐methyl‐O‐methyl‐carbamate (metabolite I), N‐phenyl‐N’ ‐formyl‐urea (metabolite II), two unstable metabolites giving (p‐chlorophenyl)‐isocyanate upon purification (metabolites III and IV), N‐(p‐chlorophenyl)‐N’ ‐methyl‐N’ ‐isobutenylol‐urea (metabolite V), p‐chloroformanilide (metabolite VI) and biologically bound p‐chloroaniline (metabolite VII). In the root and basal stem extract, the following metabolites were identified by gas chromatography/mass spectrometry: N‐(p‐chlorophenyl)‐O‐methyl‐carbamate (metabolite VIII) and N‐(p‐chlorophenyl)‐N’ ‐methyl‐urea (metabolite IX). 相似文献
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Nada Barakat Dimitris P. Makris Panagiotis Kefalas Elefteria Psillakis 《Environmental Chemistry Letters》2010,8(3):271-275
Olive mill waste water (OMWW) originating from a two-phase olive oil-producing plant was treated with a crude peroxidase extract prepared from onion solid by-products. The treatments were based on a 3 × 3 factorial design, employing a series of combinations of pH and H2O2, in order to identify optimal operational conditions. The treatment performance was assessed by estimating the removal percentage of total polyphenols. The model established produced a satisfactory fitting of the data (R 2 = 0.94, p = 0.0158), while the second-order polynomial equation used to describe the process indicated that peroxidase-catalysed polyphenol removal in diluted OMWW is facilitated at relatively low pH and intermediate H2O2 values. A predicted value of 50.7 ± 9.5% removal was calculated under optimal operational conditions (pH 2.76, [H2O2] = 3.56 mM). Analysis of an untreated and an optimally treated sample by high performance liquid chromatography revealed that enzyme treatment brought about alteration in the original OMWW polyphenolic profile. The use of peroxidase from onion solid by-products is proposed as an alternative means that could have a prospect in bioremediation applications. 相似文献
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Claire Brussol Matthew Duane Patrick Carlier Dimitrios Kotzias 《Environmental science and pollution research international》1999,6(3):138-140
The photo-induced degradation of naphthalene, 1,4-naphthoquinone, 1-naphthol and 1-NO2 naphthalene, adsorbed on silica gel, and with the addition of nitrogenous air pollutants e.g. NO2 (as KNO2) was investigated. Results indicate that compounds adsorbed onto a solid carrier are degraded when irradiated with UV light
(λ > 290 nm) in the presence of nitrites. The key species initiating the naphthalene degradation is the OH-radical which is
generated through the photolysis of NO2. Reaction products identified were 2-formyl-cinnamaldehyde, 1,4-naphthoquinone, nitronaphthol, o-phthaldialdehyde, phthalide
and nitronaphthalene. A mass balance between 40–50% was achieved. Under the same irradiation conditions, 1-NO2 naphthalene is mainly degraded by direct photolysis while degradation of 1-naphthol and 1,4-naphthoquinone proceeds via the
reaction with OH-radicals. Identified products were hydroxy-nitro-nitroso- and quinones compounds. 相似文献
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