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建立DPX快速吸附萃取、程序升温(PTV)大体积进样与气相色谱/质谱(GC/MS)联用,SIM模式同时测定水中19种多溴联苯(PBBs)单体的方法。该方法在PBBs质量浓度1~50μg/L范围内线性良好,19种PBBs单体检出限为0.147~0.230μg/L,相对标准偏差为6.61%~10.5%,加标回收率为61.5%~82.6%。 相似文献
243.
环境中苯并(a)芘监测技术及建议 总被引:1,自引:0,他引:1
环境中BaP是引起人们各类癌症的主要诱发物.叙述了环境中BaP的来源及其浓度状况,列举了国家制定的各项标准中的BaP含量的浓度限值,论述了环境水中和空气中BaP的样品采集、保存、前处理、分析测定及定量监测中应注意的几个问题,提出了监测BaP的4点建议. 相似文献
244.
简述了塔山水库蓝藻暴发的过程及成因。指出 ,由于水库的营养物质增多、水质恶化 ,在不利的水文、气象 (高温、光照充足、微风 )等条件下 ,导致蓝藻暴发。提出了相应的控制对策 相似文献
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Seasonal variation of polycyclic aromatic hydrocarbons in soil and air of Dalian areas, China: an assessment of soil-air exchange 总被引:1,自引:0,他引:1
The seasonal variations of concentrations of PAHs in the soil and the air were measured in urban and rural region of Dalian, China in 2007. In soil, mean concentrations of all PAHs in summer were larger than those in winter, whereas the concentrations of heavier weight PAHs in winter were larger than those in summer. Winter/summer concentration ratios for individual PAHs (R(W/S)) increased with the increase of molecular weight of PAHs in soil, indicating that PAHs with high molecular weight were more easily deposited to soil in winter than summer. In air, mean concentrations of all PAHs in winter were larger than those in summer. In comparison with the R(W/S) in soil, all the values of R(W/S) in air were larger than one indicating that the entire individual PAH concentrations in winter were larger than those in summer. The average concentration composition for each PAH compound in soil and air samples was determined and the seasonal change of PAH profile was very small. It was suggested that PAHs in soils and air had the same or similar sources both in winter and summer. The approach to the soil-air equilibrium was assessed by calculating fugacity quotients between soil and air using the soil and air concentrations. The calculated soil-air fugacity quotients indicated that soil acted as a secondary source to the atmosphere for all lighter weight PAHs (two-three rings) and it will continue to be a sink for heavier weight PAHs (five-six rings) in the Dalian environment, both in winter and summer. Medium weight PAHs (four-five rings) were close to the soil-air equilibrium and the tendency shifted between soil and air when season or function region changed. The fugacity quotients of PAHs in summer (mean temperature 298 K) were larger than those in winter (mean temperature 273 K), indicating a higher tendency in summer than winter for PAHs to move from soil to air. The variation of ambient conditions such as temperature, rainfall, etc. can influence the movement of PAHs between soil and air. Most of the fugacity quotients of PAHs for the urban sites were larger than that for the rural site both in winter and summer. This phenomenon may be related with that the temperatures in urban sites were higher than those in the rural site because of the urban heat island effect. 相似文献
246.
Yan Zhang Wei Luo Junmei Jia Peiru Kong Xiaojuan Tong Yonglong Lu Liqiong Xie Fulong Ma John P. Giesy 《Environmental monitoring and assessment》2014,186(8):5297-5306
Pig manure (PM) is widely used as an organic fertilizer to increase yields of crops. Excessive application of compost containing relatively great concentrations of copper (Cu) and zinc (Zn) can change soil quality. To clarify the effects of different rates of application and to determine the optimal rate of fertilization, PM containing 1,115 mg Cu kg?1, dry mass (dm) and 1,497 mg Zn kg?1, dm was applied to alkaline soil at rates of 0, 11, 22, 44, 88, and 222 g PM kg?1, dm. Phospholipid fatty acids (PLFAs) were used to assess soil microbial community composition. Application of PM resulted in greater concentrations of total nitrogen (TN), NH4 +-N, NO3 ?-N, total carbon (TC), soil organic matter (SOM) but lesser pH values. Soils with application rates of 88–222 g PM kg?1, dm had concentrations of total and EDTA-extractable Cu and Zn significantly greater than those in soil without PM, and concentrations of T-Cu and T-Zn in these amended soils exceeded maximum limits set by standards in china. Except in the soil with a rate of 11 g PM kg?1, dm, total bacterial and fungal PLFAs were directly proportional to rate of application of PM. Biomasses of bacteria and fungi were significantly greater in soils with application rates of 44–222 g PM kg?1, dm than in the soil without PM. SOM, TC and EDTA-Zn had the most direct influence on soil microbial communities. To improve fertility of soils and maintain quality of soil, rate of application should be 22–44 g PM kg?1 dm, soil containing Cu and Zn. 相似文献
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249.
在则木河断裂带宏观研究的基础上,结合岩石破裂实验成果,对包括1850年大震变形带在内的断裂产物进行定向原态采集、固结、制片和镜下系统观测,从复杂纷呈的变形遗迹中鉴别出微观粘滑与蠕滑标志。最后就有关问题进行了简要讨论. 相似文献