SPE-PDA/FLD串联HPLC法测定水样中痕量多环芳烃

建立了固相萃取-PDA/FLD串联HPLC法测定水样中多环芳烃(PAHs)的分析方法,优化了固相萃取条件.结果表明,对1L水样加入10%有机改性剂进行固相萃取,采用3ml四氢呋喃洗脱后进行HPLC分析,平均回收率在95.22%-100.8%间,相对标准偏差为0.78%-6.68%,方法的检出限在0.03-220 ng·l-1之间.     

钾细菌在剩余污泥资源化中的应用

通过对钾细菌在剩余污泥中的接种,利用钾细菌将土壤中难溶性钾转化为可溶性钾是增加作物钾素营养的一个途径,将含大量钾细菌的剩余污泥制成的微生物肥料应用于农田中,从而达到剩余污泥的资源化利用,为剩余污泥的科学处理提供依据。     

济南市环境、社会、经济协调发展评价

建立了济南市城市环境、社会、经济协调评价指标体系,采用多目标二级决策方法对各指标的权重进行分配;在已有协调度计算方法的基础上,构建了协调度的计算公式;并运用该指标体系和协调度公式对济南市环境、社会经济协调状况进行评判。结果表明济南市的环境、社会经济之间发展是不平衡的,协调状况为中级协调水平;环境综合指数较低,表明环境的建设滞后于社会经济的发展。     

脉冲法对隔声屏障顶端式样的衍射分析

介绍了声屏障顶部结构衍射的评价标准和计算方法。给出了具有T型、橄榄型、弧型、L型等4种不同顶端式样声屏障的衍射声场有限元分析,以及使用脉冲方法得到的各种顶端式样在隔声屏障铺设吸声材料和不铺设吸声材料两种情况下插入损失的计算结果。     

千层底复兴运动

大凡圣人,都喜欢云游四方,在行走中思考,在思考中进取.周游列国,纵横天下,既是一种阅历,又是一种经验.不管足上是布鞋还是朝靴,他们就这样一路走来,坦荡而又自信.     

Synthesis of a three-dimensional network sodium alginate–poly(acrylic acid)/attapulgite hydrogel with good mechanic property and reusability for efficient adsorption of Cu2+ and Pb2+

Environmental Chemistry Letters - Water pollution caused by heavy metals has dramatically impacted ecosystems in recent years. For instance, 45.4% of lakes in China are in the category of moderate...     

物元分析法在大气监测优化布点中的应用

探讨了物元分析法在大气监测优化布点中的应用，获得了符合实际情况的优选闰，证明该法简便实用。为学趺同监测部门科学合理地设置大气监测点位提供了有益的参考。     

磨料水射流除鳞技术在钢厂的应用

为了暴露各种钢材在热轧过程中产生的表面缺陷，需清除附于其上的氧化铁皮，称之为“除鳞”。传统的除鳞方法有酸洗、表面剥皮、喷丸处理等，这些方法存在很多缺点。本文介绍已在湖南涟钢用于生产的磨料水射流除鳞生产线，用磨料水射流除鳞具有速度快、质量高、成本低、操作简便等独特的优点。     

Temporal variation and spatial distribution of PAH in water of Three Gorges Reservoir during the complete impoundment period

Bioavailable concentrations of polycyclic aromatic hydrocarbons (PAHs) were investigated in water of Three Gorges Reservoir (TGR) using semipermeable membrane devices during the period of completely impounding water. ∑PAH concentrations in water of TGR in the period of completely impounding water were 15–381 ng?L^?1. ∑PAH concentrations increased from town or counties to big industrialized cities in TGR, indicating urbanization effects on PAH pollution in the water. Tributaries in TGR have a certain contribution of PAH pollution to the mainstream of Yangtze River and their pollution could not be neglected. An obvious decrease of PAH concentration was observed after 175-m water impounding in 2011 in TGR. Several factors may account for this decrease, including execution of comprehensive treatment and management measures in TGR, less rainfall in 2011, and sedimentation effect caused by the dam. Passive sampling method has been successfully applied in the investigation of trace PAH in water of TGR and proved to be a useful and efficient tool for the management and sustainable development of the big reservoir. The results of the study provide valuable information about PAH pollution in the whole reservoir including some tributaries, and the pollution status is dynamically related with human activities. Therefore, PAH could be used as a marker compound or indicator in the network monitoring system to surveil and trace the pollution status in TGR.     

Specific antibody for pesticide residue determination produced by antibody-pesticide complex

A new method for specific antibody production was developed using antibody (Ab)-pesticide complex as a unique immunogen. Parathion (PA) was the targeted pesticide, and rabbit polyclonal antibody (Pab) and mouse monoclonal antibody (Mab) were used as carrier proteins. The Ab-PA complexes were generated by conjugating the two antibodies with an excessive dosage of PA. It was shown that the sensitivity of homologous enzyme-linked immunosorbent assay (ELISA) using the new antibodies was similar to that using original antibodies. However, the new mouse Pab had not only similar positive recognizing spectrum as the original Mab, but also a significantly improved sensitivity in heterologous ELISA when some recognizable competitors were applied. IC₅₀ value of ELISA based on a combination of the new mouse Pab and hapten 9 was 0.24 ng/mL, which was 445.54 times as that of the homologous ELISA. An Ab-pesticide complex may be a suitable alternative immunogen for producing highly specific antibody to improve the immunoassay sensitivity.