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经过消解前加入氢氧化钠和改用聚四氟乙烯消化管等方面的改进,碱性过硫酸钾氧化-钼酸铵分光度法的实际操作更简便,更适用于各类水样的监测。它具有较低的捡出限(O.004mg/L),较高的精密度(RSD=1.1%)和较好的准确度(测定标样溶液相对误差1.6%,加标回收率为97.2%-102.1%)。测定IERM测量审核样的结果也较好(取得了合格证书)。不确定度的评定依照相关标准的原则进行,并使用残差来量化曲线不碹定度分量,减少了工作量。经评定,改进方法的扩展不确定度为3.2%。 相似文献
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环境空气SO2采样由每天采样3次,每次采样30分钟的瞬时采样变成24小时的连续采样,其测定浓度都降低了。其原因主要有,监测点位重新布设后,有些采样点位向郊区转移、进气管接胶管采样、进气管有水、采样流量变小及延迟化验分析等,都影响采样结果。 相似文献
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Effects of hydrocarbon compositions on raw exhaust emissions and combustion processes were studied on an engine test bench. The
optimization of gasoline hydrocarbon composition was discussed. As olefins content increased from 10.0% to 25.0% in volume, the
combustion duration was shortened by about 2 degree crank angle ( CA), and the engine-out THC emission was reduced by about 15%.
On the other hand, as aromatics content changed from 35.0% to 45.0%, the engine-out NOx emissions increased by 4%. An increment
in olefins content resulted in a slight increase in engine-out CO emission, while the aromatics content had little e ect on engine-out total
hydrocarbon (THC) and CO emissions. Over the new European driving cycle (NEDC), the THC, NOx and CO emissions of fuel with
25.0% olefins and 35.0% aromatics were about 45%, 21% and 19% lower than those of fuel with 10.0% olefins and 40.0% aromatics,
respectively. The optimized gasoline compositions for new engines and new vehicles have low aromatics and high olefins contents. 相似文献
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Evaluation of mercury speciation and removal through air pollution control
devices of a 190 MW boiler 总被引:1,自引:0,他引:1
Chengli Wu Yan Cao Zhongbing Dong Chinmin Cheng Hanxu Li Weiping Pan 《环境科学学报(英文版)》2010,22(2):277-282
Air pollution control devices (APCDs) are installed at coal-fired power plants for air pollutant regulation. Selective catalytic reduction
(SCR) and wet flue gas desulfurization (FGD) systems have the co-benefits of air pollutant and mercury removal. Configuration
and operational conditions of APCDs and mercury speciation a ect mercury removal e ciently at coal-fired utilities. The Ontario
Hydro Method (OHM) recommended by the U.S. Environmental Protection Agency (EPA) was used to determine mercury speciation
simultaneously at five sampling locations through SCR-ESP-FGD at a 190 MW unit. Chlorine in coal had been suggested as a factor
a ecting the mercury speciation in flue gas; and low-chlorine coal was purported to produce less oxidized mercury (Hg2+) and more
elemental mercury (Hg0) at the SCR inlet compared to higher chlorine coal. SCR could oxidize elemental mercury into oxidized
mercury when SCR was in service, and oxidation e ciency reached 71.0%. Therefore, oxidized mercury removal e ciency was
enhanced through a wet FGD system. In the non-ozone season, about 89.5%–96.8% of oxidized mercury was controlled, but only
54.9%–68.8% of the total mercury was captured through wet FGD. Oxidized mercury removal e ciency was 95.9%–98.0%, and there
was a big di erence in the total mercury removal e ciencies from 78.0% to 90.2% in the ozone season. Mercury mass balance was
evaluated to validate reliability of OHM testing data, and the ratio of mercury input in the coal to mercury output at the stack was from
0.84 to 1.08. 相似文献