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61.
62.
A gas chromatographic method that uses solid-phase microextraction for analysis of organic marker compounds in fine particulate matter (PM2.5) is reported. The target marker compounds were selected for specificity toward emission from wood smoke, diesel or gasoline combustion, or meat cooking. Temperature-programmed volatilization analysis was used to characterize the thermal stabilities and volatile properties of the compounds of interest. The compounds were thermally evaporated from a quartz filter, sorbed to a solid phase microextraction (SPME) fiber, and thermally desorbed at 280 degrees C in a gas chromatograph injection port connected via a DB 1701 capillary separating column. Various experimental parameters (fiber type, time, and temperature of sorption) were optimized. It was found that high extraction yield could be achieved using a polyacrylate fiber for polar substances, such as levoglucosan, and a 7-microm polydimethylsiloxane (PDMS)-coated fiber for nonpolar compounds, such as hopanes and polyaromatic hydrocarbon. A compromise was made by selecting a carboxen/PDMS fiber, which can simultaneously extract all of the analytes of interest with moderate-to-high efficiency at 180 degrees C within a 30-min accumulation period. The optimized method was applied to the determination of levoglucosan in pine wood combustion emissions. The simplicity, rapidity, and selectivity of sample collection with a polymer-coated SPME coupled to capillary gas chromatography (GC) made this method potentially useful for atmospheric chemistry studies. 相似文献
63.
Dario A. Levaggi Milton Feldstein 《Journal of the Air & Waste Management Association (1995)》2013,63(5):312-313
Formaldehyde, acrolein, and low molecular weight aldehydes are collected in 1% NaHSO3 solution in Greenberg-Smith or midget impingers from industrial effluents. Efficiency of collection is excellent when two impingers are used in series. Formaldehyde is measured in an aliquot of the collection medium by the chromo-tropic acid procedure, acrolein by a modified mercuric-chloride-hexylresorcinol procedure, and C2-C5 aldehydes by a gas chromatographic procedure. The method permits the analysis of all C1-C5 aldehydes on a single collection sample. Data on aldehyde concentrations from a variety of effluents are presented. 相似文献
64.
65.
Terry W. Rothermel Milton S. Sachs Frank O'Shaughnessy 《Journal of the American Water Resources Association》1971,7(4):867-877
ABSTRACT The Office of Saline Water, which has federal responsibility for developing low-cost, saline sources of fresh water, has recognized the need for an improved method of forecasting the future potential of desalting in this country. The magnitude of the role of desalting will influence the plans of federal, state, and local water resource agencies and the research and development programs of manufacturers. A dynamic simulation model has been developed by Arthur D. Little, Inc. under contract by OSW to translate relevant factors of water supply and demand into a forecast of desalting potential. The model projects the needs for desalting in 20 hydrologic regions of the U.S. Model performance has thus far been demonstrated by the development of a forecast and a battery of related sensitivity tests. Current results indicate the following potential desalting capacities: 225 MGD in 1980; 2,250 MGD in 2000; and 7,000 MGD in 2020. Significant improvements in desalting economics promise to increase these potentials by a factor of four or five by 2000-2020. Model inputs and results are continuing to be refined. When completed, OSW will have a dynamic tool with which to guide its R&D program. 相似文献
66.
67.
Potassium, phosphorus, or nitrogen limit root allocation, tree growth, or litter production in a lowland tropical forest 总被引:5,自引:0,他引:5
Wright SJ Yavitt JB Wurzburger N Turner BL Tanner EV Sayer EJ Santiago LS Kaspari M Hedin LO Harms KE Garcia MN Corre MD 《Ecology》2011,92(8):1616-1625
We maintained a factorial nitrogen (N), phosphorus (P), and potassium (K) addition experiment for 11 years in a humid lowland forest growing on a relatively fertile soil in Panama to evaluate potential nutrient limitation of tree growth rates, fine-litter production, and fine-root biomass. We replicated the eight factorial treatments four times using 32 plots of 40 x 40 m each. The addition of K was associated with significant decreases in stand-level fine-root biomass and, in a companion study of seedlings, decreases in allocation to roots and increases in height growth rates. The addition of K and N together was associated with significant increases in growth rates of saplings and poles (1-10 cm in diameter at breast height) and a further marginally significant decrease in stand-level fine-root biomass. The addition of P was associated with a marginally significant (P = 0.058) increase in fine-litter production that was consistent across all litter fractions. Our experiment provides evidence that N, P, and K all limit forest plants growing on a relatively fertile soil in the lowland tropics, with the strongest evidence for limitation by K among seedlings, saplings, and poles. 相似文献