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61.
A solid phase extraction method for the determination of gold(III) at trace levels by flame atomic absorption spectrometer
(FAAS) was developed. The method was based on retention of gold as chloro complexes through the Amberlite XAD-2000. The effect
of some analytical parameters including hydrochloric acid concentration, sample volume, sample and eluent flow rates, eluent
volume, eluent concentration and interfering ions on the recovery of gold(III) was investigated. The retention of gold(III)
from 1.5 mol l−1 HCl solution and the recovery of gold with 0.07 mol l−1 NH3 solution were quantitative (≥95%). The relative standard deviation (RSD) was calculated as 3.2% (n = 10). The detection limit for gold was 2 μg l−1. The accuracy was checked with the determination of gold spiked an artificial seawater and a pure copper samples. 相似文献
62.
Contamination levels of selected organochlorine and organophosphate pesticides in the Selangor River, Malaysia between 2002 and 2003 总被引:3,自引:0,他引:3
In Malaysia, rivers are the main source of public water supplies. This study was conducted from 2002 to 2003 to determine the levels of selected organochlorine and organophosphate pesticides in the Selangor River in Malaysia. Surface water samples have been collected seasonally from nine sites along the river. A liquid-liquid extraction followed by gas chromatography-mass spectrometry technique was used to determine the trace levels of these pesticide residues. The organochlorine pesticides detected were lindane, heptachlor, endosulfan, dieldrin, endosulfan sulfate, o,p'-DDT, p,p'-DDT, o,p'-DDE and p,p'-DDE whereas for organophosphate pesticides, they were chlorpyrifos and diazinon. At the river upstream where a dam is located for public water supply, incidents of pesticide levels exceeding the European Economic Community Directive of water quality standards have occurred. Furthermore, the wetland ecosystems located at the downstream of the river which houses the fireflies community is being threatened by occasional pesticide levels above EPA limits for freshwater aquatic organisms. The occurrence of these residual pesticides in the Selangor River can be attributed to the intense agriculture and urban activity. 相似文献
63.
64.
Alginate encapsulated nano-hydroxyapatite beads were synthesized and characterized by Fourier transform infrared spectroscopy, Brunauer–Emmett–Teller surface analysis, and X-ray diffraction. Their adsorptive potential for Ni2+ and rhodamine B was explored in batch mode and by fixed-bed column passage. In the batch system, maximum uptake capacity for Ni2+ was 360 mg g?1 and 480 mg g?1 for rhodamine B. In the presence of humic acid, sorption was enhanced. For the continuous-flow system, adsorption was effective at low flow rate. For both pollutants, mass transport resistance increased during adsorption. The overall rates of rhodamine B and Ni2+ uptake were found to be controlled by external mass transfer. 相似文献
65.
Determination of heavy metals in lower Sakarya river sediments using a BCR-sequential extraction procedure 总被引:1,自引:0,他引:1
Dundar MS Altundag H Eyupoglu V Keskin SC Tutunoglu C 《Environmental monitoring and assessment》2012,184(1):33-41
A BCR-sequential extraction procedure for the determination of extractable heavy metals was applied to sediments of various
rivers and lakes. There are many rivers basins in Turkey. Sakarya River Basin is one of the most important basins, which consists
of three parts: Upper, Middle and Lower Sakarya River Basins. In this study, the Lower Sakarya River was selected as the study
area for sediments. The samples were collected monthly from 10 pre-determined stations through the river for 10 months time
and analysed for the distribution of Cd, Co, Cr, Cu, Fe, Mn, Ni, Pb and Zn elements. The determination of extractable heavy
metals in sediments was carried out by using Flame Atomic Absorption Spectrometer. The validation of the results was performed
by the analysis of a BCR 701 standard reference material. 相似文献
66.
Silva Neicí Cáceres Poetini Márcia Rósula Bianchini Matheus Chimelo Almeida Francielli Polet Dahle Mustafá Munir Mustafa Araujo Stífani Machado Bortolotto Vandreza Cardoso Musachio Elize Aparecida Santos Ramborger Bruna Piaia Novo Diogo La Rosa Roehrs Rafael Mesko Marcia Foster Prigol Marina Puntel Robson Luiz 《Environmental science and pollution research international》2021,28(14):17519-17531
Environmental Science and Pollution Research - Manganese (Mn) is an essential element that, in excess, seems to be involved in the development of different neurodegenerative conditions.... 相似文献
67.
Melik Kara Yetkin Dumanoğlu Hasan Altıok Tolga Elbir Mustafa Odabası Abdurrahman Bayram 《Environmental monitoring and assessment》2014,186(10):6017-6038
Topsoil samples (n?=?40) were collected from a heavily industrialized region in Turkey. The region includes several scrap processing iron–steel plants with electric arc furnaces (EAFs), a petroleum refinery, a petrochemical complex, steel rolling mills, a natural gas-fired power plant, ship-breaking yards and very dense transportation activities. The region has undergone a rapid transition from an agricultural region to a heavily industrialized region in the last three decades. Collected soil samples were analyzed for 48 trace elements using inductively coupled plasma-mass spectrometry (ICP-MS). The elemental distribution pattern in the region indicated that Nemrut area with dense iron–steel production activities was a hotspot for elemental pollution. In addition to crustal elements, concentrations of anthropogenic trace elements (i.e., Fe, Zn, Pb, Mn, Cu, Cd, Cr and Mo) were very high in the area influencing many parts of the region. Elemental compositions of fugitive sources polluting the soil (i.e., paved and unpaved roads, slag piles, EAFs filter dust piles and coal piles) were also determined. The methods (enrichment factors [EFs] and the index of geoaccumulation [I geo]) used for determination of pollution status of soil showed that Cr, Ag, Zn, As and Pb were the strongly contaminating elements for the region. Principal component analysis (PCA) clearly indicated that anthropogenic sources (steel production, refinery and petrochemical processes and traffic) were important sources in this region. 相似文献
68.
69.
The rate of heavy metal pollution in some minor fruit samples growing at roadsides in Turkey were determined by inductively
coupled plasma-atomic emission spectrometry (ICP-AES). The mineral contents of samples were found to be different depending
on the several parts Citrus fruits. The highest minor and heavy metal levels for Citrus fruits were determined between 17.24 and 45.30 mg/kg boron, 2.08 and 15.05 mg/kg copper, 1.01 and 16.00 mg/kg iron and 2.35
and 9.87 mg/kg zinc. Boron content ranged from 16.54 mg/kg (Deveci pear inner pulp) to 89.89 mg/kg (Arjantin apple outer skin).
The level of Fe ranged from 1.49 mg/kg (quince pulp) to 25.05 mg/kg (Ankara pear pulp). Cu content of fruits ranged between
2.52 mg/kg (Fuji apple skin) and 25.93 mg/kg quince skin). Zn content was found between 0.46 mg/kg (Golden apple pulp) and
14.34 mg/kg (quince skin). P contents ranged from 651 mg/kg (Golden apple pulp) to 1269 mg/kg (quince skin). Na was found
between 500 mg/kg (Fuji apple skin) and 907 mg/kg (Arjantin apple skin). 相似文献
70.