Quantification of human amniotic fluid constituents by high resolution proton nuclear magnetic resonance (NMR) spectroscopy

We have investigated the ability of high-resolution proton NMR spectroscopy to provide a biochemical constituent screening of human amniotic fluid (AF). Proton NMR spectra were obtained at 300 MHz on AF from patients undergoing amniocentesis in the mid-trimester. Only AF from normal pregnancies (normal fetal karyotype, normal a-fetoprotein levels, normal birth outcome) was used in this study. The AF supernatant was lyophilized and resuspended in deuterated water containing 0.1 mm phosphate buffer and 6.02 mm disodium maleate. Identification of low molecular weight compounds was confirmed by two-dimensional NMR spectra (primarily correlated spectroscopy, or COSY) and standard addition techniques. A broad profile of compounds were ‘NMR visible’ in a single proton spectrum, including creatinine, glucose, organic acids (acetate, citrate, and lactate) and several amino acids (alanine, histidine, leucine, phenylalanine, tyrosine and valine). The proton spectrum was unaffected by prior freezing/thawing of AF samples. We were able to quantify compounds by comparison with an added concentration standard (maleate) at concentrations as low as 30 μm. Good agreement with literature values based on other analytical techniques was obtained.     

Der Strahlungshaushalt der terrestrischen Planeten Venus,Erde und Mars

The radiation budget of planets substantially determines their climates. For the terrestrial planets having their own imperceptible heat source compared to the solar radiation, the radiation budget supplies energy that can be transformed and used in their atmospheres and at their surfaces. The crucial role of the radiation budget for the Earth's climate is manifested in current international programs like the World Climate and Global Change Programs. The intercomparison and analysis of the radiation budget of the terrestrial planets, due to quite different atmospheric compositions and external conditions, provide a deeper insight into the relations of the different components of the radiation budget.     

全封闭垃圾焚烧空气污染影响与控制措施

以大坦沙资源电厂为研究对象 ,通过对全封闭垃圾燃烧、污染物去除、废气高空排放工艺流程分析以及运用列举法和大气扩散数学模式对全封闭垃圾焚烧厂的污染影响与控制进行了探究 ,提出了有关垃圾焚烧空气污染防治对策和建议 ,为垃圾焚烧处理提供参考     

AutoCAD环境下压铸模模板图形库系统设计

采用AutoCAD及其内部语言AutoLISP ,在AutoCAD环境下 ,开发了压铸模模板图形库系统。利用本系统只需输入几个基本参数 ,即可生成压铸模模板图形及相应的零件图。