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181.
Maja A. Shishovska Vera P. Trajkovska Marina T. Stefova 《Journal of environmental science and health. Part. B》2013,48(7):694-701
An isocratic High Performance Liquid Chromatographic (HPLC) method was optimized for 3-phenoxybenzyl (1RS)-cis-trans-3-(2,2-dichlorovinyl)-2,2-dimethyl-cyclopropanecarboxylate (permethrin) residues identification and quantification in wine matrix. Analytical reverse phase (RP) C-18 column was used (25 cm × 4 mm i.d., 5 μ m) with mobile phase consisting of acetonitrile and water in ratio 70 %/30 % (v v?1), flow-rate 2.0 mL min?1, UV-detection at 215 nm and controlled oven temperature at 25°C. The peaks of isomers were identified with the retention times as compared to standard cis-/trans- mixture and confirmed with characteristic spectra using photodiode array detector. Under these conditions, permethrin isomers were well separated with resolution 2.8 and no interference with the naturally present wine compounds was observed. The method was validated for linearity, precision, accuracy, limit of detection (LOD) and limit of quantification (LOQ). Linear regression analysis data proved a good linear relationship (correlation coefficients, r2, for cis- and trans-isomer are: 0.9995 and 0.9997, respectively) between response of the detector and concentration of permethrin isomers over a wide concentration range for both isomers (0.55 mg L?1 ?4.40 mg L?1). Experimental data showed mean recoveries between 93.95% and 96.58% with RSD values in range: 0.89% ?3.69%. The effect of ethanol content in the solvent on permethrin isomers peak areas was also studied and 60% v v?1 ethanol was found to be optimal for sample preparation. The method was successfully tested on 20 commercial wine samples from the market in which no permethrin was detected. Thus, it was proved that it is suitable for routine permethrin residues analysis. The proposed method is suitable for routine analysis because of the simple sample preparation, acceptable run-time, low cost and its applicability with conventional instruments. 相似文献
182.
Several investigations were carried out on biotic and abiotic samples to determine the difference between Chernobyl and preChernobyl environmental radiocontamination of the Adriatic Sea. Special emphasis was put on the determination of 137Cs which resulted in the most abundant radionuclide in a wide variety of samples (sea water, sediment, pelagic and benthic species). Attention was also given to the neutron activation products 110mAg and 134Cs that were first discovered in the Adriatic ecosystem after the Chernobyl event in particular, although the 110Ag fallout deposition over the area was neglected in comparison to that of 137Cs, its bioaccumulation in macroalgae and molluscs was much higher suggesting some particular physiological accumulation mechanism. 相似文献
183.
Marina?Fontaine Alice?Carravieri Beno?t?Simon-Bouhet Paco?Bustamante Nicolas?Gasco Frédéric?Bailleul Christophe?Guinet Yves?CherelEmail author 《Marine Biology》2015,162(1):207-219
The food and feeding ecology of the poorly known southern long-finned pilot whale (Globicephala melas edwardii) was investigated using ecological tracers (muscle and skin δ13C and δ15N, and total mercury, Hg) on individuals from two mass strandings together with at-sea observations of live animals in Kerguelen waters, southern Indian Ocean. Sightings of cetaceans from longliners over 9 years (2003–2012) emphasized the regular occurrence of pilot whales in slope waters surrounding the archipelago. Tissue δ13C values (a proxy of consumer foraging habitat) suggest that pilot whales fed in slope waters and in oceanic subantarctic waters over the last months preceding stranding. Tissue δ15N values and Hg concentration (dietary proxies) indicate a high trophic position (~4.7) for the pilot whales, likely corresponding to a mixed diet of fish and squid (not crustaceans) of undetermined species. Both skin and muscle Hg concentrations were positively and linearly correlated to individual size with no concomitant δ15N changes, which can be interpreted as a progressive Hg accumulation in tissues of individuals throughout life with no parallel dietary shift. Skin and muscle Hg concentrations were linearly and positively related; hence, Hg skin could be used as a proxy of Hg concentration in muscle (a main Hg reservoir of the body). Kerguelen southern long-finned pilot whales were less Hg contaminated than most pilot whale populations studied so far, thus suggesting that they are not at a high risk to Hg-induced damages in the remote islands of the Southern Ocean. 相似文献
184.
Chiara Chiapponi Enrico Pavoni Barbara Bertasi Laura Baioni Erika Scaltriti Edoardo Chiesa Luca Cianti Marina Nadia Losio Stefano Pongolini 《Food and environmental virology》2014,6(3):202-206
Hepatitis A virus (HAV) was detected in two samples of mixed frozen berries linked to Italian hepatitis A outbreak in April and September 2013. Both viruses were fully sequenced by next-generation sequencing and the genomes clustered with HAV complete genomes of sub-genotype IA with nucleotide identities of 95–97 %. 相似文献
185.
Multiple exposure pathways and health risk assessment of selenium for children in a coal mining area
dos Santos Marina Ramires Paula Florêncio Gironés María Consuelo Revert Rubio Armendáriz María del Carmen Montelongo Soraya Paz Muccillo-Baisch Ana Luíza da Silva Junior Flavio Manoel Rodrigues 《Environmental science and pollution research international》2021,28(11):13562-13569
Environmental Science and Pollution Research - Selenium (Se) presents a dual role to human body, harmful or beneficial, depending on its concentration. The exposure to this element has been... 相似文献
186.
Montano Luigi Donato Francesco Bianco Pietro Massimiliano Lettieri Gennaro Guglielmino Antonino Motta Oriana Bonapace Ian Marc Piscopo Marina 《Environmental science and pollution research international》2021,28(28):37031-37040
Environmental Science and Pollution Research - The epidemic of the new severe acute respiratory syndrome coronavirus 2 (SARS-CoV-2) has impacted worldwide with its infectious spread and mortality... 相似文献
187.
188.
M. Carla de Aranzamendi Ricardo Sahade Marcos Tatián Marina B. Chiappero 《Marine Biology》2008,154(5):875-885
The limpet Nacella concinna (Strebel 1908) was the focus of numerous studies dealing with Antarctic benthos. One of the main characteristics of the species
is the presence of two distinguishable morphotypes, one inhabiting the intertidal (during summer) and the other inhabiting
the subtidal. For a long time these forms were considered as an expression of phenotypic plasticity, since previous studies
did not found genetic differences between them. In the present work, we performed both a morphometric and a genetic differentiation
analysis (using ISSR-PCR markers) of these two forms in three stations sampled at Potter Cove, South Shetland Islands. The
results confirmed the morphological differences between intertidal and subtidal forms reported in other Antarctic localities.
The genetic differences detected indicate that the two forms can be considered as genetically distinct populations maintaining
low levels of gene flow. The degree of reproductive isolation of the ecotypes is discussed, as well as the possible origin
of the divergence. The genetic differentiation observed can also have behavioral and physiological correlates, pointing out
the importance of taking into account the potential differences in the response of both populations to different conditions
in future studies in this species.
M. C. de Aranzamendi and R. Sahade contributed equally to this paper. 相似文献
189.
190.
Silvana Povolo Maria Giovanna Romanelli Federico Fontana Marina Basaglia Sergio Casella 《Journal of Polymers and the Environment》2012,20(4):944-949
The production of polyesters from triglyceride containing substrates was investigated. A first filter step based on lipase activity was followed and those bacteria potentially able to degrade oils or animal fats were further tested for their polymer accumulation properties, selected and kept for further studies. In a second step, bacteria were directly grown on animal fats and/or vegetable oils, and polyhydroxyalkanoates (PHAs) accumulation was verified under appropriate incubation conditions. Each substrate, whether of animal or vegetable derivation, supported the growth of a number of the newly isolated strains and among those, some strains were also found to produce reasonably high amounts of PHA. The repeat-unit composition of the polyesters was determined by gas chromatography (GC) analysis of the ?-hydroxyalkanoate methyl esters from the hydrolyzed polymer and some class of co-polymers were also detected. These properties, coupled with the ability of some of the selected isolates to grow and produce lipases on a minimal medium, could be considered as promising in view of possible industrial applications. The overall results indicate that PHAs could be produced from waste containing considerable amounts of fat, oil and grease (FOG), that generally need to be treated for their disposal. 相似文献